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19 "Polymerization shrinkage"
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Evaluation of polymerization shrinkage stress in silorane-based composites
Seung-Ji Ryu, Ji-Hoon Cheon, Jeong-Bum Min
J Korean Acad Conserv Dent 2011;36(3):188-195.   Published online May 31, 2011
DOI: https://doi.org/10.5395/JKACD.2011.36.3.188
AbstractAbstract PDFPubReaderePub
Objectives

The purpose of this study was to evaluate the polymerization shrinkage stress among conventional methacrylate-based composite resins and a silorane-based composite resin.

Materials and Methods

The strain gauge method was used for the determination of polymerization shrinkage strain. Specimens were divided by 3 groups according to various composite materials. Filtek Z-250 (3M ESPE) and Filtek P-60 (3M ESPE) were used as a conventional methacrylate-based composites and Filtek P-90 (3M ESPE) was used as a silorane-based composites. Measurements were recorded at each 1 second for the total of 800 seconds including the periods of light application. The results of polymerization shrinkage stress were statistically analyzed using One way ANOVA and Tukey test (p = 0.05).

Results

The polymerization shrinkage stress of a silorane-based composite resin was lower than those of conventional methacrylate-based composite resins (p < 0.05). The shrinkage stress between methacrylate-based composite resin groups did not show significant difference (p > 0.05).

Conclusions

Within the limitation of this study, silorane-based composites showed lower polymerization shrinkage stress than methacrylate-based composites. We need to investigate more into polymerization shrinkage stress with regard to elastic modulus of silorane-based composites for the precise result.

Citations

Citations to this article as recorded by  
  • Polymerization shrinkage and stress analysis during dental restoration observed by digital image correlation method
    Jung-Hoon Park, Nak-Sam Choi
    Journal of Mechanical Science and Technology.2021; 35(12): 5435.     CrossRef
  • Evaluation of the color stability of light cured composite resins according to the resin matrices
    Da-Hye Yu, Hyun-Jin Jung, Sung-Hyeon Choi, In-Nam Hwang
    Korean Journal of Dental Materials.2019; 46(2): 109.     CrossRef
  • Behavior of Polymerization Shrinkage Stress of Methacrylate-based Composite and Silorane-based Composite during Dental Restoration
    Jung-Hoon Park, Nak-Sam Choi
    Composites Research.2015; 28(1): 6.     CrossRef
  • Microtensile bond strength of silorane-based composite specific adhesive system using different bonding strategies
    Laura Alves Bastos, Ana Beatriz Silva Sousa, Brahim Drubi-Filho, Fernanda de Carvalho Panzeri Pires-de-Souza, Lucas da Fonseca Roberti Garcia
    Restorative Dentistry & Endodontics.2015; 40(1): 23.     CrossRef
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A new method to measure the linear polymerization shrinkage of composites using a particle tracking method with computer vision
In-Bog Lee, Sun-Hong Min, Deog-Gyu Seo, Sun-Young Kim, Youngchul Kwon
J Korean Acad Conserv Dent 2010;35(3):180-187.   Published online May 31, 2010
DOI: https://doi.org/10.5395/JKACD.2010.35.3.180
AbstractAbstract PDFPubReaderePub

Since the introduction of restorative dental composites, their physical properties have been significantly improved. However, polymerization shrinkage is still a major drawback. Many efforts have been made to develop a low shrinking composite, and silorane-based composites have recently been introduced into the market. In addition, many different methods have been developed to measure the polymerization shrinkage.

In this study, we developed a new method to measure the linear polymerization shrinkage of composites without direct contact to a specimen using a particle tracking method with computer vision. The shrinkage kinetics of a commercial silorane-based composite (P90) and two conventional methacrylate-based composites (Z250 and Z350) were investigated and compared. The results were as follows:

The linear shrinkage of composites was 0.33-1.41%. Shrinkage was lowest for the silorane-based (P90) composite, and highest for the flowable Z350 composite.

The new instrument was able to measure the true linear shrinkage of composites in real time without sensitivity to the specimen preparation and geometry.

Citations

Citations to this article as recorded by  
  • Effect of layering methods, composite type, and flowable liner on the polymerization shrinkage stress of light cured composites
    Youngchul Kwon, Jack Ferracane, In-Bog Lee
    Dental Materials.2012; 28(7): 801.     CrossRef
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Effect of the exponential curing of composite resin on the microtensile dentin bond strength of adhesives
So-Rae Seong, Duck-kyu Seo, In-Bog Lee, Ho-Hyun Son, Byeong-Hoon Cho
J Korean Acad Conserv Dent 2010;35(2):125-133.   Published online March 31, 2010
DOI: https://doi.org/10.5395/JKACD.2010.35.2.125
AbstractAbstract PDFPubReaderePub
Objectives

Rapid polymerization of overlying composite resin causes high polymerization shrinkage stress at the adhesive layer. In order to alleviate the shrinkage stress, increasing the light intensity over the first 5 seconds was suggested as an exponential curing mode by an LED light curing unit (Elipar FreeLight2, 3M ESPE). In this study, the effectiveness of the exponential curing mode on reducing stress was evaluated with measuring microtensile bond strength of three adhesives after the overlying composite resin was polymerized with either continuous or exponential curing mode.

Methods

Scotchbond Multipurpose Plus (MP, 3M ESPE), Single Bond 2 (SB, 3M ESPE), and Adper Prompt (AP, 3M ESPE) were applied onto the flat occlusal dentin of extracted human molar. The overlying hybrid composite (Denfil, Vericom, Korea) was cured under one of two exposing modes of the curing unit. At 48h from bonding, microtensile bond strength was measured at a crosshead speed of 1.0 mm/min. The fractured surfaces were observed under FE-SEM.

Results

There was no statistically significant difference in the microtensile bond strengths of each adhesive between curing methods (Two-way ANOVA, p > 0.05). The microtensile bond strengths of MP and SB were significantly higher than that of AP (p < 0.05). Mixed failures were observed in most of the fractured surfaces, and differences in the failure mode were not observed among groups.

Conclusion

The exponential curing method had no beneficial effect on the microtensile dentin bond strengths of three adhesives compared to continuous curing method.

Citations

Citations to this article as recorded by  
  • The effect of the strength and wetting characteristics of Bis-GMA/TEGDMA-based adhesives on the bond strength to dentin
    Eun-Sook Park, Chang-Keun Kim, Ji-Hyun Bae, Byeong-Hoon Cho
    Journal of Korean Academy of Conservative Dentistry.2011; 36(2): 139.     CrossRef
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Polymerization shrinkage kinetics of silorane-based composites
Youngchul Kwon, In-Bog Lee
J Korean Acad Conserv Dent 2010;35(1):51-58.   Published online January 31, 2010
DOI: https://doi.org/10.5395/JKACD.2010.35.1.051
AbstractAbstract PDFPubReaderePub

Dental composites have improved significantly in physical properties over the past few decades. However, polymerization shrinkage and stress is still the major drawback of composites, limiting its use to selected cases. Much effort has been made to make low shrinking composites to overcome this issue and silorane-based composites have recently been introduced into the market.

The aim of this study was to measure the volumetric polymerization shrinkage kinetics of a silorane-based composite and compare it with conventional methacrylate-based composites in order to evaluate its effectiveness in reducing polymerization shrinkage.

Five commercial methacrylate-based (Beautifil, Z100, Z250, Z350 and Gradia X) and a silorane-based (P90) composites were investigated. The volumetric change of the composites during light polymerization was detected continuously as buoyancy change in distilled water by means of Archemedes'principle, using a newly made volume shrinkage measurement instrument. The null hypothesis was that there were no differences in polymerization shrinkage, peak polymerization shrinkage rate and peak shrinkage time between the silorane-based composite and methacrylate-based composites. The results were as follows:

The shrinkage of silorane-based (P90) composites was the lowest (1.48%), and that of Beautifil composite was the highest (2.80%). There were also significant differences between brands among the methacrylate-based composites.

Peak polymerization shrinkage rate was the lowest in P90 (0.13%/s) and the highest in Z100 (0.34%/s).

The time to reach peak shrinkage rate of the silorane-based composite (P90) was longer (6.7 s) than those of the methacrylate-based composites (2.4-3.1 s).

Peak shrinkage rate showed a strong positive correlation with the product of polymerization shrinkage and the inverse of peak shrinkage time (R = 0.95).

Citations

Citations to this article as recorded by  
  • Comparison of polymerization shrinkage of dual-cure core build-up resin according to shade and curing mode
    Yoorina Choi, Karl Lee, Hoon-Sang Chang
    Oral Biology Research.2019; 43(4): 243.     CrossRef
  • Evaluation of polymerization shrinkage stress in silorane-based composites
    Seung-Ji Ryu, Ji-Hoon Cheon, Jeong-Bum Min
    Journal of Korean Academy of Conservative Dentistry.2011; 36(3): 188.     CrossRef
  • A new method to measure the linear polymerization shrinkage of composites using a particle tracking method with computer vision
    In-Bog Lee, Sun-Hong Min, Deog-Gyu Seo, Sun-Young Kim, Youngchul Kwon
    Journal of Korean Academy of Conservative Dentistry.2010; 35(3): 180.     CrossRef
  • 211 View
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  • 3 Crossref
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Original Articles
Effect of fiber direction on the polymerization shrinkage of fiber-reinforced composites
Joongwon Yom, In-Bog Lee
J Korean Acad Conserv Dent 2009;34(4):364-370.   Published online July 31, 2009
DOI: https://doi.org/10.5395/JKACD.2009.34.4.364
AbstractAbstract PDFPubReaderePub

The aim of this study was to evaluate the effect of fiber direction on the polymerization shrinkage of fiber-reinforced composite. The disc-shaped flowable composite specimens (d = 10 mm, h = 2 mm, Aeliteflo A2, Bisco, Inc., IL, USA) with or without glass fiber bundle (X-80821P Glass Fiber, Bisco, Inc., IL, USA) inside were prepared, and the longitudinal and transversal polymerization shrinkage of the specimens on radial plane were measured with strain gages (Linear S-series 350ω, CAS, Seoul, Korea). In order to measure the free polymerization shrinkage of the flowable composite itself, the disc-shaped specimens (d = 7 mm, h = 1 mm) without fiber were prepared, and the axial shrinkage was measured with an LVDT (linear variable differential transformer) displacement sensor. The cross-section of the polymerized specimens was observed with a scanning electron microscope to examine the arrangement of the fiber bundle in composite. The mean polymerization shrinkage value of each specimen group was analyzed with ANOVA and Scheffe post-hoc test (α=0.05).

The radial polymerization shrinkage of fiber-reinforced composite was decreased in the longitudinal direction of fiber, but increased in the transversal direction of fiber (p<0.05). We can conclude that the polymerization shrinkage of fiber-reinforced composite splint or restoratives is dependent on the direction of fiber.

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Effect of instrument compliance on the polymerization shrinkage stress measurements of dental resin composites
Deog-Gyu Seo, Sun-Hong Min, In-Bog Lee
J Korean Acad Conserv Dent 2009;34(2):145-153.   Published online March 31, 2009
DOI: https://doi.org/10.5395/JKACD.2009.34.2.145
AbstractAbstract PDFPubReaderePub

The purpose of this study was to evaluate the effect of instrument compliance on the polymerization shrinkage stress measurements of dental composites. The contraction strain and stress of composites during light curing were measured by a custom made stress-strain analyzer, which consisted of a displacement sensor, a cantilever load cell and a negative feedback mechanism. The instrument can measure the polymerization stress by two modes: with compliance mode in which the instrument compliance is allowed, or without compliance mode in which the instrument compliance is not allowed.

A flowable (Filtek Flow: FF) and two universal hybrid (Z100: Z1 and Z250: Z2) composites were studied. A silane treated metal rod with a diameter of 3.0 mm was fixed at free end of the load cell, and other metal rod was fixed on the base plate. Composite of 1.0 mm thickness was placed between the two rods and light cured. The axial shrinkage strain and stress of the composite were recorded for 10 minutes during polymerization, and the tensile modulus of the materials was also determined with the instrument. The statistical analysis was conducted by ANOVA, paired t-test and Tukey's test (α<0.05).

There were significant differences between the two measurement modes and among materials. With compliance mode, the contraction stress of FF was the highest: 3.11 (0.13), followed by Z1: 2.91 (0.10) and Z2: 1.94 (0.09) MPa. When the instrument compliance is not allowed, the contraction stress of Z1 was the highest: 17.08 (0.89), followed by FF: 10.11 (0.29) and Z2: 9.46 (1.63) MPa. The tensile modulus for Z1, Z2 and FF was 2.31 (0.18), 2.05 (0.20), 1.41 (0.11) GPa, respectively. With compliance mode, the measured stress correlated with the axial shrinkage strain of composite; while without compliance the elastic modulus of materials played a significant role in the stress measurement.

Citations

Citations to this article as recorded by  
  • Effects of cuspal compliance and radiant emittance of LED light on the cuspal deflection of replicated tooth cavity
    Chang-Ha LEE, In-Bog LEE
    Dental Materials Journal.2021; 40(3): 827.     CrossRef
  • Polymerization Shrinkage and Stress of Silorane-based Dental Restorative Composite
    In-Bog Lee, Sung-Hwan Park, Hyun-Jeong Kweon, Ja-Uk Gu, Nak-Sam Choi
    Composites Research.2013; 26(3): 182.     CrossRef
  • Evaluation of polymerization shrinkage stress in silorane-based composites
    Seung-Ji Ryu, Ji-Hoon Cheon, Jeong-Bum Min
    Journal of Korean Academy of Conservative Dentistry.2011; 36(3): 188.     CrossRef
  • The change of the initial dynamic visco-elastic modulus of composite resins during light polymerization
    Min-Ho Kim, In-Bog Lee
    Journal of Korean Academy of Conservative Dentistry.2009; 34(5): 450.     CrossRef
  • 164 View
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Effect of intermittent polymerization on the rate of polymerization shrinkage and cuspal deflection in composite resin
Min Kyung Kim, Sung Ho Park, Deog Gyu Seo, Yun Jung Song, Yoon Lee, Chan Young Lee
J Korean Acad Conserv Dent 2008;33(4):341-351.   Published online July 31, 2008
DOI: https://doi.org/10.5395/JKACD.2008.33.4.341
AbstractAbstract PDFPubReaderePub

This study investigated the effect of intermittent polymerization on the rate of polymerization shrinkage and cuspal deflection in composite resins.

The linear polymerization shrinkage of each composite was measured using the custom-made linometer along with the light shutter specially devised to block the light at the previously determined interval. Samples were divided into 4 groups by light curing method; Group 1) continuous light (60s with light on); Group 2) intermittent light (cycles of 3s with 2s light on & 1s with light off for 90s); Group 3) intermittent light (cycles of 2s with 1s light on & 1s with light off for 120s); Group 4) intermittent light (cycles of 3s with 1s light on & 2s with light off for 180s). The amount of linear polymerization shrinkage was measured and its maximum rate (Rmax) and peak time (PT) in the first 15 seconds were calculated. For the measurement of cuspal deflection of teeth, MOD cavities were prepared in 10 extracted maxillary premolars. Reduction in the intercuspal distance was measured by the custom-made cuspal deflection measuring machine. ANOVA analysis was used for the comparison of the light curing groups and t-test was used to determine significant difference between the composite resins.

Pyramid showed the greater amount of polymerization shrinkage than Heliomolar (p < 0.05). There was no significant difference in the linear polymerization shrinkage among the groups. The Rmax was group 4 < 3, 2 < 1 in Heliomolar and group 3 < 4 < 2, 1 in Pyramid (p < 0.05). Pyramid demonstrated greater cuspal deflection than Heliomolar. The cuspal deflection in Heliomolar was group 4 < 3 < 2, 1 and group 4, 3 < 2, 1 in Pyramid (p < 0.05).

It was concluded that the reduced rate of polymerization shrinkage by intermittent polymerization can help to decrease the cuspal deflection.

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Polymerization shrinkage, hygroscopic expansion and microleakage of resin-based temporary filling materials
Nak Yeon Cho, In-Bog Lee
J Korean Acad Conserv Dent 2008;33(2):115-124.   Published online March 31, 2008
DOI: https://doi.org/10.5395/JKACD.2008.33.2.115
AbstractAbstract PDFPubReaderePub

The purpose of this study was to measure the polymerization shrinkage and hygroscopic expansion of resin-based temporary filling materials and to evaluate microleakage at the interface between the materials and cavity wall.

Five resin-based temporary filing materials were investigated: Fermit (Vivadent), Quicks (Dentkist), Provifil (Promedica), Spacer (Vericom), Clip (Voco). Caviton (GC) was also included for comparison. Polymerization shrinkage of five resin-based temporary filling materials was measured using the bonded disc method. For the measurement of hygroscopic expansion, the discs of six cured temporary filling materials were immersed in saline and a LVDT displacement sensor was used to measure the expansion for 7 days. For estimating of microleakage, Class I cavities were prepared on 120 extracted human molars and randomly assigned to 6 groups of 20 each. The cavities in each group were filled with six temporary filling materials. All specimens were submitted to 1000 thermo-cycles, with temperature varying from 5℃/55℃. Microleakage was determined using a dye penetration test.

The results were as follows:

Fermit had significantly less polymerization shrinkage than the other resin-based temporary filling materials. Fermit (0.22 %) < Spacer (0.38 %) < Quicks (0.64 %), Provifil (0.67 %), Clip (0.67 %)

Resin-based temporary filling materials showed 0.43 - 1.1 % expansion in 7 days.

Fermit showed the greatest leakage, while Quicks exhibited the least leakage.

There are no correlation between polymerization shrinkage or hygroscopic expansion and microleakage of resin-based temporary filling materials.

Citations

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  • Comparison of color stability, gloss, mechanical and physical properties according to dental temporary filling materials type
    Ji-Won Choi, You-Young Shin, Song-Yi Yang
    Korean Journal of Dental Materials.2022; 49(3): 97.     CrossRef
  • Comparative analysis of strain according to two wavelengths of light source and constant temperature bath deposition in ultraviolet-curing resin for dental three-dimensional printing
    Dong-Yeon Kim, Gwang-Young Lee, Hoo-Won Kang, Cheon-Seung Yang
    Journal of Korean Acedemy of Dental Technology.2020; 42(3): 208.     CrossRef
  • Effect of cavity disinfectants on antibacterial activity and microtensile bond strength in class I cavity
    Bo-Ram KIM, Man-Hwan OH, Dong-Hoon SHIN
    Dental Materials Journal.2017; 36(3): 368.     CrossRef
  • Shear bond strength of a self-adhesive resin cement to resin-coated dentin
    Jee-Youn Hong, Cheol-Woo Park, Jeong-Uk Heo, Min-Ki Bang, Jae-Jun Ryu
    The Journal of Korean Academy of Prosthodontics.2013; 51(1): 27.     CrossRef
  • Coronal microleakage of four temporary restorative materials in Class II-type endodontic access preparations
    Sang-Mi Yun, Lorena Karanxha, Hee-Jin Kim, Sung-Ho Jung, Su-Jung Park, Kyung-San Min
    Restorative Dentistry & Endodontics.2012; 37(1): 29.     CrossRef
  • Microtensile bond strength of resin inlay bonded to dentin treated with various temporary filling materials
    Tae-Woo Kim, Bin-Na Lee, Young-Jung Choi, So-Young Yang, Hoon-Sang Chang, Yun-Chan Hwang, In-Nam Hwang, Won-Mann Oh
    Journal of Korean Academy of Conservative Dentistry.2011; 36(5): 419.     CrossRef
  • The Effect of Temporary Filling Materials on The Adhesion between Dentin Adhesive-coated Surface and Resin Inlay
    Tae-Gun Kim, Kwang-Won Lee, Mi-Kyung Yu
    Journal of Korean Academy of Conservative Dentistry.2008; 33(6): 553.     CrossRef
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Cuspal deflection in class V cavities restored with composite resins
Jun-Gyu Park, Bum-Soon Lim, In-Bog Lee
J Korean Acad Conserv Dent 2008;33(2):83-89.   Published online March 31, 2008
DOI: https://doi.org/10.5395/JKACD.2008.33.2.083
AbstractAbstract PDFPubReaderePub

The purpose of this study was to evaluate the effect of the polymerization shrinkage and modulus of elasticity of composites on the cusp deflection of class V restoration in premolars. The sixteen extracted upper premolars were divided into 2 groups with similar size. The amounts of cuspal deflection were measured in Class V cavities restored with a flowable composite (Filtek flow) or a universal hybrid composite (Z-250). The bonded interfaces of the sectioned specimens were observed using a scanning electron microscopy (SEM). The polymerization shrinkage and modulus of elasticity of the composites were measured to find out the effect of physical properties of composite resins on the cuspal deflection. The results were as follows.

The amounts of cuspal deflection restored with Filtek flow or Z-250 were 2.18 ± 0.92 µm and 2.95 ± 1.13 µm, respectively. Filtek flow showed less cuspal deflection but there was no statistically significant difference (p > 0.05).

The two specimens in each group showed gap at the inner portion of the cavity.

The polymerization shrinkages of Filtek flow and Z-250 were 4.41% and 2.23% respectively, and the flexural modulus of elasticity of cured Filtek flow (7.77 GPa) was much lower than that of Z-250 (17.43 GPa).

The cuspal deflection depends not only on the polymerization shrinkage but also on the modulus of elasticity of composites.

Citations

Citations to this article as recorded by  
  • Comparison of marginal microleakage between low and high flowable resins in class V cavity
    Sang-Bae Bae, Young-Gon Cho, Myeong-Seon Lee
    Journal of Korean Academy of Conservative Dentistry.2009; 34(6): 477.     CrossRef
  • A survey on the use of composite resin in Class II restoration in Korea
    Dong-Ho Shin, Se-Eun Park, In-Seok Yang, Juhea Chang, In-Bog Lee, Byeong-Hoon Cho, Ho-Hyun Son
    Journal of Korean Academy of Conservative Dentistry.2009; 34(2): 87.     CrossRef
  • Effect of instrument compliance on the polymerization shrinkage stress measurements of dental resin composites
    Deog-Gyu Seo, Sun-Hong Min, In-Bog Lee
    Journal of Korean Academy of Conservative Dentistry.2009; 34(2): 145.     CrossRef
  • The change of the initial dynamic visco-elastic modulus of composite resins during light polymerization
    Min-Ho Kim, In-Bog Lee
    Journal of Korean Academy of Conservative Dentistry.2009; 34(5): 450.     CrossRef
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Effect of a new resin monomer on the microleakage of composite resin restorations
JH Bae, YK Kim, PY Yoon, MA Lee, BH Cho
J Korean Acad Conserv Dent 2007;32(5):469-475.   Published online September 30, 2007
DOI: https://doi.org/10.5395/JKACD.2007.32.5.469
AbstractAbstract PDFPubReaderePub

The purpose of this study was to evaluate the effect of a new resin monomer on the microleakage of composite resin restorations. By adding new methoxylated Bis-GMA (Bis-M-GMA, 2,2-bis[4-(2-methoxy-3-methacryloyloxy propoxy) phenyl] propane) having low viscosity, the content of TEGDMA which has adverse effects on polymerization shrinkage might be decreased. As a result, microleakage might be improved.

2 mm × 2 mm × 2 mm cavities with occlusal margins in enamel and gingival margins in dentin were prepared on buccal and lingual surfaces of 40 extracted human premolars. Prepared teeth were randomly divided into four groups and restored with Clearfil SE bond (Kuraray, Japan) and one of experimental composite resins; EX1, Experimental composite resin1 (Bis-M-GMA/TEGDMA = 95/5 wt%, 40 nm nanofillers); EX2, Experimental composite resin2 (Bis-M-GMA/TEGDMA = 95/5 wt%, 20 nm nanofillers); EX3, Experimental composite resin3 (Bis-GMA/TEGDMA = 70/30 wt%, 40 nm nanofillers); and Filtek Z250 (3M ESPE, USA) was filled as a control group. The restored teeth were thermocycled, and immersed in 2% methylene blue solution for 24 hours. The teeth were sectioned buccolingually with a low speed diamond saw and evaluated for microleakage under stereomicroscope. The data were statistically analyzed by Pearson Chi-Square test and Fisher Exact test (p = 0.05).

The microleakage scores seen at the enamel margin were significantly lower than those of dentin margin (p = 0.007). There were no significant differences among the composite resins in the microleakage scores within each margin (p > 0.05). Bis-M-GMA, a new resin monomer having low viscosity, might in part replace high viscous Bis-GMA and might improve the quality of composite resin.

Citations

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  • Sealing Ability of Three Different Materials Used as Retrograde Filling
    Ji-Hoon Park, Seung-Bok Kang, Yong-Hoon Choi, Ji-Hyun Bae
    Journal of Korean Dental Science.2012; 5(2): 60.     CrossRef
  • Surface roughness of experimental composite resins using confocal laser scanning microscope
    JH Bae, MA Lee, BH Cho
    Journal of Korean Academy of Conservative Dentistry.2008; 33(1): 1.     CrossRef
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The effect of intermittent composite curing on marginal adaptation
Yong-Hwan Yun, Sung-Ho Park
J Korean Acad Conserv Dent 2007;32(3):248-259.   Published online May 31, 2007
DOI: https://doi.org/10.5395/JKACD.2007.32.3.248
AbstractAbstract PDFPubReaderePub

The aim of this research was to study the effect of intermittent polymerization on marginal adaptation by comparing the marginal adaptation of intermittently polymerized composite to that of continuously polymerized composite.

The materials used for this study were Pyramid (Bisco Inc., Schaumburg, U.S.A.) and Heliomolar (Ivoclar Vivadent, Liechtenstein). The experiment was carried out in class II MOD cavities prepared in 48 extracted human maxillary premolars. The samples were divided into 4 groups by light curing method; group 1- continuous curing (60s light on with no light off); group 2- intermittent curing (cycles of 3s with 2s light on & 1s light off for 90s); group 3- intermittent curing (cycles of 2s with 1s light on & 1s light off for 120s); group 4- intermittent curing (cycles of 3s with 1s light on & 2s light off for 180s). Consequently the total amount of light energy radiated was same in all the groups. Each specimen went through thermo-mechanical loading (TML) which consisted of mechanical loading (720,000 cycles, 5.0 kg) with a speed of 120 rpm for 100 hours and thermocycling (6000 thermocycles of alternating water of 50℃ and 55℃). The continuous margin (CM) (%) of the total margin and regional margins, occlusal enamel (OE), vertical enamel (VE), and cervical enamel (CE)) was measured before and after TML under a × 200 digital light microscope.

Three-way ANOVA and Duncan's Multiple Range Test was performed at 95% level of confidence to test the effect of 3 variables on CM (%) of the total margin: light curing conditions, composite materials and effect of TML. In each group, One-way ANOVA and Duncan's Multiple Range Test was additionally performed to compare CM (%) of regions (OE, VE, CE).

The results indicated that all the three variables were statistically significant (p < 0.05). Before TML, in groups using Pyramid, groups 3 and 4 showed higher CM (%) than groups 1 and 2, and in groups using Heliomolar, groups 3 and 4 showed higher CM (%) than group 1 (p < 0.05). After TML, in both Pyramid and Heliomolar groups, group 3 showed higher CM (%) than group 1 (p < 0.05). CM (%) of the regions are significantly different in each group (p < 0.05). Before TML, no statistical difference was found between groups within the VE and CE region. In the OE region, group 4 of Pyramid showed higher CM (%) than group 2, and groups 2 and 4 of Heliomolar showed higher CM (%) than group 1 (p < 0.05). After TML, no statistical difference was found among groups within the VE and CE region. In the OE region, group 3 of Pyramid showed higher CM (%) than groups 1 and 2, and groups 2,3 and 4 of Heliomolar showed higher CM (%) than group 1 (p < 0.05).

It was concluded that intermittent polymerization may be effective in reducing marginal gap formation.

Citations

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  • Effect of the exponential curing of composite resin on the microtensile dentin bond strength of adhesives
    So-Rae Seong, Duck-kyu Seo, In-Bog Lee, Ho-Hyun Son, Byeong-Hoon Cho
    Journal of Korean Academy of Conservative Dentistry.2010; 35(2): 125.     CrossRef
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Polymerization shrinkage of composite resins cured by variable light intensities
Mi-Young Lim, Kyung-Mo Cho, Chan-Ui Hong
J Korean Acad Conserv Dent 2007;32(1):28-36.   Published online January 31, 2007
DOI: https://doi.org/10.5395/JKACD.2007.32.1.028
AbstractAbstract PDFPubReaderePub

The purpose of this study was to compare the effect of exponential curing method with conventional curing and soft start curing method on polymerization shrinkage of composite resins.

Three brands of composite resins (Synergy Duo Shade, Z250, Filtek Supreme) and three brands of light curing units (Spectrum 800, Elipar Highlight, Elipar Trilight) were used. 40 seconds curing time was given. The shrinkage was measured using linometer for 90 seconds.

The effect of time on polymerization shrinkage was analysed by one-way ANOVA and the effect of curing modes and materials on polymerization shrinkage at the time of 90s were analysed by two-way ANOVA. The shrinkage ratios at the time of 20s to 90s were taken and analysed the same way. The results were as follows:

1. All the groups except Supreme shrank almost within 20s. Supreme cured by soft start and exponential curing had no further shrinkage after 30s (p < 0.05).

2. Statistical analysis revealed that polymerization shrinkage varied among materials (p = 0.000) and curing modes (p = 0.003). There was no significant interaction between material and curing mode.

3. The groups cured by exponential curing showed the statistically lower polymerization shrinkage at 90s than the groups cured by conventional curing and soft start curing (p < 0.05).

4. The initial shrinkage ratios of soft start and exponential curing were statistically lower than conventional curing (p < 0.05).

From this study, the use of low initial light intensities may reduce the polymerization rate and, as a result, reduce the stress of polymerization shrinkage.

Citations

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  • Degree of Conversion and Polymerization Shrinkage of Low and High Viscosity Bulk-Fill Giomer-based and Resin-based composites
    Heera Kim, Jaesik Lee, Hyunjung Kim, Taeyub Kwon, Soonhyeun Nam
    THE JOURNAL OF THE KOREAN ACADEMY OF PEDTATRIC DENTISTRY.2019; 46(1): 1.     CrossRef
  • Effect of the exponential curing of composite resin on the microtensile dentin bond strength of adhesives
    So-Rae Seong, Duck-kyu Seo, In-Bog Lee, Ho-Hyun Son, Byeong-Hoon Cho
    Journal of Korean Academy of Conservative Dentistry.2010; 35(2): 125.     CrossRef
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The effect of C-factor and volume on microleakage of composite resin restorations with enamel margins
Bong-Joo Koo, Dong-Hoon Shin
J Korean Acad Conserv Dent 2006;31(6):452-459.   Published online November 30, 2006
DOI: https://doi.org/10.5395/JKACD.2006.31.6.452
AbstractAbstract PDFPubReaderePub

Competition will usually develop between the opposing walls as the restorative resin shrinks during polymerization. Magnitude of this phenomenon may be depended upon cavity configuration and volume.

The purpose of this sturdy was to evaluate the effect of cavity configuration and volume on microleakage of composite resin restoration that has margins on the enamel site only.

The labial enamel of forty bovine teeth was ground using a model trimmer to expose a flat enamel surface. Four groups with cylindrical cavities were defined, according to volume and configuration factor (Depth × Diameter / C-factor) - Group I: 1.5 mm × 2.0 mm / 4.0, Group II: 1.5 mm × 6.0 mm / 2.0, Group III: 2.0 mm × 1.72 mm / 5.62, Group IV: 2.0 mm × 5.23 mm / 2.54.

After treating with fifth-generation one-bottle adhesive - BC Plus™ (Vericom, AnYang, Korea), cavities were bulk filled with microhybrid composite resin - Denfill™ (Vericom). Teeth were stored in distilled water for one day at room temperature and were finished and polished with Sof-Lex system. Specimens were thermocycled 500 times between 5℃ and 55℃ for 30 second at each temperature.

Teeth were isolated with two layers of nail varnish except the restoration surface and 1 mm surrounding margins. Electrical conductivity (µA) was recorded in distilled water by electrochemical method. Microleakage scores were compared and analyzed using two-way ANOVA at 95% level.

The results were as follows:

1. Small cavity volume showed lower microleakage score than large one, however, there was no statistically significant difference.

2. There was no relationship between cavity configuration and microleakage.

Factors of cavity configuration and volume did not affect on microleakage of resin restorations with enamel margins only.

Citations

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  • Influence of rebonding procedures on microleakage of composite resin restorations
    Mi-Ae Lee, Duck-Kyu Seo, Ho-Hyun Son, Byeong-Hoon Cho
    Journal of Korean Academy of Conservative Dentistry.2010; 35(3): 164.     CrossRef
  • Microleakage of the experimental composite resin with three component photoinitiator systems
    Ji-Hoon Kim, Dong-Hoon Shin
    Journal of Korean Academy of Conservative Dentistry.2009; 34(4): 333.     CrossRef
  • A survey on the use of composite resin in Class II restoration in Korea
    Dong-Ho Shin, Se-Eun Park, In-Seok Yang, Juhea Chang, In-Bog Lee, Byeong-Hoon Cho, Ho-Hyun Son
    Journal of Korean Academy of Conservative Dentistry.2009; 34(2): 87.     CrossRef
  • Difference in bond strength according to filling techniques and cavity walls in box-type occlusal composite resin restoration
    Eun-Joo Ko, Dong-Hoon Shin
    Journal of Korean Academy of Conservative Dentistry.2009; 34(4): 350.     CrossRef
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Effect of cavity shape, bond quality and volume on dentin bond strength
Hyo-Jin Lee, Jong-Soon Kim, Shin-Jae Lee, Bum-Soon Lim, Seung-Ho Baek, Byeong-Hoon Cho
J Korean Acad Conserv Dent 2005;30(6):450-460.   Published online November 30, 2005
DOI: https://doi.org/10.5395/JKACD.2005.30.6.450
AbstractAbstract PDFPubReaderePub

The aim of this study was to evaluate the effect of cavity shape, bond quality of bonding agent and volume of resin composite on shrinkage stress developed at the cavity floor. This was done by measuring the shear bond strength with respect to iris materials (cavity shape; adhesive-coated dentin as a high C-factor and Teflon-coated metal as a low C-factor), bonding agents (bond quality; Scotchbond™ Multi-purpose and Xeno®III) and iris hole diameters (volume; 1 mm or 3 mm in diameter × 1.5 mm in thickness). Ninety-six molars were randomly divided into 8 groups (2 × 2 × 2 experimental setup). In order to simulate a Class I cavity, shear bond strength was measured on the flat occlusal dentin surface with irises. The iris hole was filled with Z250 restorative resin composite in a bulk-filling manner. The data was analyzed using three-way ANOVA and the Tukey test. Fracture mode analysis was also done. When the cavity had high C-factor, good bond quality and large volume, the bond strength decreased significantly. The volume of resin composite restricted within the well-bonded cavity walls is also be suggested to be included in the concept of C-factor, as well as the cavity shape and bond quality. Since the bond quality and volume can exaggerate the effect of cavity shape on the shrinkage stress developed at the resin-dentin bond, resin composites must be filled in a method, which minimizes the volume that can increase the C-factor.

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Correlation between Linear polymerization shrinkage & tooth cuspal deflection
Soon-Young Lee, Sung-Ho Park
J Korean Acad Conserv Dent 2005;30(6):442-449.   Published online November 30, 2005
DOI: https://doi.org/10.5395/JKACD.2005.30.6.442
AbstractAbstract PDFPubReaderePub

The purpose of the present study was to evaluate the relationship between the amount of cuspal deflection and linear polymerization shrinkage in resin composite and polyacid modified resin composite. For cuspal defelction and shrinkage measurement, Dyract AP, Compoglass F, Z100, Surefil, Pyramid, Synergy Compact, Heliomolar and Heliomolar HB were used.

For measuring polymerization shrinkage, a custom made linometer (R&B, Daejon, Korea) was used. The amount of shrinkage among materials was compared using One-way ANOVA analysis and Tukey's test at the 95% of confidence level.

For measuring cuspal deflection of teeth, standardized MOD cavities were prepared in extracted maxillary premolars. After a self-etching adhesive was applied, cavities were bulk filled with one of the filling materials.Fifteen teeth were used for each material. Cuspal deflection was measured by a custom made cuspal-deflection measuring device. One-way ANOVA analysis and Tukey's test were used to determine differences between the materials at the 95% of confidence level.

Correlation of polymerization shrinkage and cuspal deflection were analyzed by regression analysis.

The amount of polymerization shrinkage from least to greatest was Heliomolar, Surefil < Heliomolar HB < Z100, Synergy Compact < Dyract AP < Pyramid, Compoglass F (p < 0.05).

The amount of cuspal deflection from least to greatest was Z100, Heliomolar, Heliomolar HB, Synergy Compact Surefil < Compoglass F < Pyramid, Dyract AP (p < 0.05).

The amount of polymerization shrinkage and cuspal deflection showed a correlation (p < 0.001).

Citations

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  • Comparison of Premolar Cuspal Deflection in Bulk or in Incremental Composite Restoration Methods
    ME Kim, SH Park
    Operative Dentistry.2011; 36(3): 326.     CrossRef
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Measurements of shrinkage stress and reduction of inter-cuspal distance in maxillary premolars resulting from polymerization of composites and compomers
Soon-Young Lee, Sung-Ho Park
J Korean Acad Conserv Dent 2004;29(4):346-352.   Published online July 31, 2004
DOI: https://doi.org/10.5395/JKACD.2004.29.4.346
AbstractAbstract PDFPubReaderePub

The purpose of present study was to evaluate the polymerization shrinkage stress and cuspal deflection in maxillary premolars resulting from polymerization shrinkage of composites and compomers.

Composites and compomers which were used in this study were as follows: Dyract AP, Z100, Surefil, Pyramid, Synergy Compact, Heliomolar, Heliomolar HB, and Compoglass F. For measuring of polymerization shrinkage stress, Stress measuring machine (R&B, Daejon, Korea) was used. One-way ANOVA analysis with Duncan's multiple comparison test were used to determine significant differences between the materials.

For measuring of cuspal deflection of tooth, MOD cavities were prepared in 10 extracted maxillary premolars. And reduction of intercuspal distance was measured by strain measuring machine (R&B, Daejon, Korea) One-way ANOVA analysis with Turkey test were used to determine significant differences between the materials.

Polymerization shrinkage stress is 『Heliomolar, Z100, Pyramid < Synergy Compact Compoglass F < Dyract AP < Heliomolr HB, surefil』 (P < 0.05). And cuspal delfelction is 『Z100, Heliomolar, Heliomolar HB, Synergy Compact Surefil, < Compoglass F < Pyramid, Dyract AP』 (P < 0.05).

Measurements of ploymerization shrinkage stress and those of cuspal deflection of the teeth was different. There is no correlation between polymerization shrinkage stress and cuspal deflection of the teeth (p > 0.05).

Citations

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  • Influence of thermal and thermomechanical stimuli on a molar tooth treated with resin-based restorative dental composites
    Jerrin Thadathil Varghese, Behzad Babaei, Paul Farrar, Leon Prentice, B. Gangadhara Prusty
    Dental Materials.2022; 38(5): 811.     CrossRef
  • Effect of intermittent polymerization on the rate of polymerization shrinkage and cuspal deflection in composite resin
    Min Kyung Kim, Sung Ho Park, Deog Gyu Seo, Yun Jung Song, Yoon Lee, Chan Young Lee
    Journal of Korean Academy of Conservative Dentistry.2008; 33(4): 341.     CrossRef
  • The effect of intermittent composite curing on marginal adaptation
    Yong-Hwan Yun, Sung-Ho Park
    Journal of Korean Academy of Conservative Dentistry.2007; 32(3): 248.     CrossRef
  • Correlation Between the Amount of Linear Polymerization Shrinkage and Cuspal Deflection
    S-Y. Lee, S-H. Park
    Operative Dentistry.2006; 31(3): 364.     CrossRef
  • Correlation between Linear polymerization shrinkage & tooth cuspal deflection
    Soon-Young Lee, Sung-Ho Park
    Journal of Korean Academy of Conservative Dentistry.2005; 30(6): 442.     CrossRef
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The effect of viscosity, specimen geometry and adhesion on the linear polymerization shrinkage measurement of light cured composites
In-Bog Lee, Ho-Hyun Son, Hyuk-Chun Kwon, Chung-Moon Um, Byeong-Hoon Cho
J Korean Acad Conserv Dent 2003;28(6):457-466.   Published online November 30, 2003
DOI: https://doi.org/10.5395/JKACD.2003.28.6.457
AbstractAbstract PDFPubReaderePub
Objectives

The aim of study was to investigate the effect of flow, specimen geometry and adhesion on the measurement of linear polymerization shrinkage of light cured composite resins using linear shrinkage measuring device.

Methods

Four commercially available composites - an anterior posterior hybrid composite Z100, a posterior packable composite P60 and two flowable composites, Filtek flow and Tetric flow - were studied. The linear polymerization shrinkage of composites was determined using 'bonded disc method' and 'non-bonded' free shrinkage method at varying C-factor in the range of 1~8 by changing specimen geometry. These measured linear shrinkage values were compared with free volumetric shrinkage values.

The viscosity and flow of composites were determined and compared by measuring the dropping speed of metal rod under constant load.

Results

In non-bonded method, the linear shrinkage approximated one third of true volumetric shrinkage by isotropic contraction. However, in bonded disc method, as the bonded surface increased the linear shrinkage increased up to volumetric shrinkage value by anisotropic contraction. The linear shrinkage value increased with increasing C-factor and approximated true volumetric shrinkage and reached plateau at about C-factor 5~6. The more flow the composite was, reduced linear shrinkage was measured by compensation radial flow.

Citations

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  • Influence of cavity size and restoration methods on the cusp deflection in composite restoration
    Mi-Ra Lee, In-Bog Lee, Chang-In Seok, Sang-Tag Lee, Chung-Moon Um
    Journal of Korean Academy of Conservative Dentistry.2004; 29(6): 532.     CrossRef
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The amounts and speed of polymerization shrinkage and microhardness in LED cured composites
Sung-Ho Park, Su-Sun Kim, Yong-Sik Cho, Soon-Young Lee, Do-Hyun Kim, Yong-Joo Jang, Hyun-Sung Mun, Jung-Won Seo, Byung-Duk Noh
J Korean Acad Conserv Dent 2003;28(4):354-359.   Published online July 31, 2003
DOI: https://doi.org/10.5395/JKACD.2003.28.4.354
AbstractAbstract PDFPubReaderePub

This study evaluated the effectiveness of the light emitting diode(LED) units for composite curing. To compare its effectiveness with conventional quartz tungsten halogen (QTH) light curing unit, the microhardness of 2mm composite, Z250, which had been light cured by the LEDs (Ultralume LED2, FreeLight, Developing product D1) or QTH (XL 3000) were compared on the upper and lower surface. One way ANOVA with Tukey and Paired t-test was used at 95% levels of confidence. In addition, the amount of linear polymerization shrinkage was compared between composites which were light cured by QTH or LEDs using a custom-made linometer in 10s and 60s of light curing, and the amount of linear polymerization shrinkage was compared by one way ANOVA with Tukey.

The amount of polymerization shrinkage at 10s was

XL3000 > Ultralume 2, 40, 60> FreeLight, D1 (P<0.05)

The amount of polymerization shrinkage at 60s was

XL3000 > Ultralume 2, 60> Ultralume 2,40> FreeLight, D1 (P<0.05)

The microhardness on the upper and lower surface was as follows;

It was concluded that the LEDs produced lower polymerization shrinkage in 10s and 60s compared with QTH unit. In addition, the microhardness of samples which had been cured with LEDs was lower on the lower surfaces than the upper surfaces whereas there was no difference in QTH cured samples.

Citations

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  • The polymerization rate and the degree of conversion of composite resins by different light sources
    Joo-Hee Ryoo, In-Bog Lee, Hyun-Mee Yoo, Mi-Ja Kim, Chang-In Seok, Hyuk-Choon Kwon
    Journal of Korean Academy of Conservative Dentistry.2004; 29(4): 386.     CrossRef
  • Measurements of shrinkage stress and reduction of inter-cuspal distance in maxillary premolars resulting from polymerization of composites and compomers
    Soon-Young Lee, Sung-Ho Park
    Journal of Korean Academy of Conservative Dentistry.2004; 29(4): 346.     CrossRef
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Amount of polymerization shrinkage and shrinkage stress in composites and compomers for posterior restoration
Sung-Ho Park, Soon-Young Lee, Yong-Sik Cho, Su-Sun Kim, Chang-Jae Lee, Young-Joo Kim, Bong-Hee Lee, Kouang-Sung Lee, Byung-Duk Noh
J Korean Acad Conserv Dent 2003;28(4):348-353.   Published online July 31, 2003
DOI: https://doi.org/10.5395/JKACD.2003.28.4.348
AbstractAbstract PDFPubReaderePub

The purpose of present study was to evaluate the polymerization shrinkage stress and amount of linear shrinkage of composites and compomers for posterior restoration.

For this purpose, linear polymerization shrinkage and polymerization stress were measured.

For linear polymerization shrinklage and polymerization stress measurement, custom made Linometer (R&B, Daejon, Korea) and Stress measuring machine was used (R&B, Daejon, Korea). Compositers and compomers were evaluated; Dyract AP (Dentsply Detrey, Gumbh. German) Z100 (3M Dental Products, St. Paul, USA) Surefil (Dentsply Caulk, Milford, USA) Pyramid(Bisco, Schaumburg, USA) Synergy Compact (Coltene, Altstatten, Switzerland), Heliomolar (Vivadent/Ivoclar, Liechtenstein), and Compoglass (Vivadent Ivoclar/Liechtenstein) were used. 15 measurements were made for each material. Linear polymerization shrinkage or polymerization stress for each material was compared with one way ANOVA with Tukey at 95% levels of confidence.

For linear shrinkage; Heliomolar, Surefil<Synergy Compact, Z100<Dyract AP<Pyramid, Compoglass F (p<0.05)

For Shrinkage stress; Heliomolar<Z100, Pyramid<Synergy Compact, Compoglass F<Dyract AP<Heliomolar HB, Surefil (p<0.05)

Citations

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  • A comparative study on color and dimensional stability of esthetic indirect dental materials
    Hye-Yun Heo, Hyo-Jin Son, Yu-Ri Heo, Mee-Kyoung Son
    Oral Biology Research.2019; 43(4): 306.     CrossRef
  • Measurement of the Internal Adaptation of Resin Composites Using Micro-CT and Its Correlation With Polymerization Shrinkage
    HJ Kim, SH Park
    Operative Dentistry.2014; 39(2): e57.     CrossRef
  • Comparison of Premolar Cuspal Deflection in Bulk or in Incremental Composite Restoration Methods
    ME Kim, SH Park
    Operative Dentistry.2011; 36(3): 326.     CrossRef
  • Effect of intermittent polymerization on the rate of polymerization shrinkage and cuspal deflection in composite resin
    Min Kyung Kim, Sung Ho Park, Deog Gyu Seo, Yun Jung Song, Yoon Lee, Chan Young Lee
    Journal of Korean Academy of Conservative Dentistry.2008; 33(4): 341.     CrossRef
  • Correlation Between the Amount of Linear Polymerization Shrinkage and Cuspal Deflection
    S-Y. Lee, S-H. Park
    Operative Dentistry.2006; 31(3): 364.     CrossRef
  • Correlation between Linear polymerization shrinkage & tooth cuspal deflection
    Soon-Young Lee, Sung-Ho Park
    Journal of Korean Academy of Conservative Dentistry.2005; 30(6): 442.     CrossRef
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  • 6 Crossref
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