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Polymerization shrinkage, hygroscopic expansion and microleakage of resin-based temporary filling materials
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Original Article Polymerization shrinkage, hygroscopic expansion and microleakage of resin-based temporary filling materials
Nak Yeon Cho, In-Bog Lee
Journal of Korean Academy of Conservative Dentistry 2008;33(2):115-124.
DOI: https://doi.org/10.5395/JKACD.2008.33.2.115
Published online: March 31, 2008

Department of Consevative Dentistry, School of Dentistry, Seoul National University, Korea.

Corresponding Author: In-Bog Lee. Department of Conservative Dentistry, School of Dentistry, Seoul National University, 275-1 Yeongeon-Dong, Jongno-Gu, Seoul 110-768, Korea. Tel: 82-2-2072-3953, Fax: 82-2-2072-3859, inboglee@snu.ac.kr
• Received: January 28, 2008   • Revised: March 5, 2008   • Accepted: March 6, 2008

Copyright © 2008 Korean Academy of Conservative Dentistry

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  • The purpose of this study was to measure the polymerization shrinkage and hygroscopic expansion of resin-based temporary filling materials and to evaluate microleakage at the interface between the materials and cavity wall.
    Five resin-based temporary filing materials were investigated: Fermit (Vivadent), Quicks (Dentkist), Provifil (Promedica), Spacer (Vericom), Clip (Voco). Caviton (GC) was also included for comparison. Polymerization shrinkage of five resin-based temporary filling materials was measured using the bonded disc method. For the measurement of hygroscopic expansion, the discs of six cured temporary filling materials were immersed in saline and a LVDT displacement sensor was used to measure the expansion for 7 days. For estimating of microleakage, Class I cavities were prepared on 120 extracted human molars and randomly assigned to 6 groups of 20 each. The cavities in each group were filled with six temporary filling materials. All specimens were submitted to 1000 thermo-cycles, with temperature varying from 5℃/55℃. Microleakage was determined using a dye penetration test.
    The results were as follows:
    1. Fermit had significantly less polymerization shrinkage than the other resin-based temporary filling materials. Fermit (0.22 %) < Spacer (0.38 %) < Quicks (0.64 %), Provifil (0.67 %), Clip (0.67 %)

    2. Resin-based temporary filling materials showed 0.43 - 1.1 % expansion in 7 days.

    3. Fermit showed the greatest leakage, while Quicks exhibited the least leakage.

    4. There are no correlation between polymerization shrinkage or hygroscopic expansion and microleakage of resin-based temporary filling materials.

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Figure 1
Structure of an instrument to measure axial polymerization shrinkage.
jkacd-33-115-g001.jpg
Figure 2
Representative curves of axial polymerization shrinkage of temporary filling materials as a function of time.
jkacd-33-115-g002.jpg
Figure 3-a
Hygroscopic expansion of Caviton as a function of time.
jkacd-33-115-g003.jpg
Figure 3-b
Initial hygroscopic expansion of temporary resin materials as a function of time.
jkacd-33-115-g004.jpg
Figure 4
The representative pictures for different microleakage patterns.
(a) Score 0: no leakage
(b) Score 1: leakage up to half of the cavity depth
(c) Score 2: leakage in the entire cavity depth without reaching the pulpal wall
(d) Score 3: leakage in the entire cavity depth even reaching the pulpal wall
jkacd-33-115-g005.jpg
Figure 5
Boxplot display of mean and median leakage score for each group.
The plot illustrates a summary of the microleakage scores based on the median, quartiles, and extreme values. The box represents the interquartile range which contains the 50% of values, the whiskers represent the highest and lowest microleakage values and the bold black line across the box indicates the median microleakage scores. The mark ◇ represents the mean microleakge scores.
jkacd-33-115-g006.jpg
Table 1
Materials used in this study
jkacd-33-115-i001.jpg
Table 2
Calculated linear polymerization shrinkage (%) of temporary filling materials

The numbers in parenthesis are S.D.

Same superscript letters mean that there is no statistical difference.

Calculated linear shrinkage = measured axial shrinkage ×(1/3)

jkacd-33-115-i002.jpg
Table 3
Hygroscopic expansion (%) of temporary filling materials at 24 hr and 7 days

The numbers in parenthesis are S.D.

Same superscript letters mean that there is no statistical difference.

jkacd-33-115-i003.jpg
Table 4
Number of specimens in each score and mean microleakage score
jkacd-33-115-i004.jpg

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        Polymerization shrinkage, hygroscopic expansion and microleakage of resin-based temporary filling materials
        J Korean Acad Conserv Dent. 2008;33(2):115-124.   Published online March 31, 2008
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      Polymerization shrinkage, hygroscopic expansion and microleakage of resin-based temporary filling materials
      Image Image Image Image Image Image
      Figure 1 Structure of an instrument to measure axial polymerization shrinkage.
      Figure 2 Representative curves of axial polymerization shrinkage of temporary filling materials as a function of time.
      Figure 3-a Hygroscopic expansion of Caviton as a function of time.
      Figure 3-b Initial hygroscopic expansion of temporary resin materials as a function of time.
      Figure 4 The representative pictures for different microleakage patterns. (a) Score 0: no leakage (b) Score 1: leakage up to half of the cavity depth (c) Score 2: leakage in the entire cavity depth without reaching the pulpal wall (d) Score 3: leakage in the entire cavity depth even reaching the pulpal wall
      Figure 5 Boxplot display of mean and median leakage score for each group. The plot illustrates a summary of the microleakage scores based on the median, quartiles, and extreme values. The box represents the interquartile range which contains the 50% of values, the whiskers represent the highest and lowest microleakage values and the bold black line across the box indicates the median microleakage scores. The mark ◇ represents the mean microleakge scores.
      Polymerization shrinkage, hygroscopic expansion and microleakage of resin-based temporary filling materials

      Materials used in this study

      Calculated linear polymerization shrinkage (%) of temporary filling materials

      The numbers in parenthesis are S.D.

      Same superscript letters mean that there is no statistical difference.

      Calculated linear shrinkage = measured axial shrinkage ×(1/3)

      Hygroscopic expansion (%) of temporary filling materials at 24 hr and 7 days

      The numbers in parenthesis are S.D.

      Same superscript letters mean that there is no statistical difference.

      Number of specimens in each score and mean microleakage score

      Table 1 Materials used in this study

      Table 2 Calculated linear polymerization shrinkage (%) of temporary filling materials

      The numbers in parenthesis are S.D.

      Same superscript letters mean that there is no statistical difference.

      Calculated linear shrinkage = measured axial shrinkage ×(1/3)

      Table 3 Hygroscopic expansion (%) of temporary filling materials at 24 hr and 7 days

      The numbers in parenthesis are S.D.

      Same superscript letters mean that there is no statistical difference.

      Table 4 Number of specimens in each score and mean microleakage score


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