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HOME > Restor Dent Endod > Volume 36(3); 2011 > Article
Basic Research Evaluation of polymerization shrinkage stress in silorane-based composites
Seung-Ji Ryu, DDS, Ji-Hoon Cheon, DDS, Jeong-Bum Min, DDS, PhD
2011;36(3):-195.
DOI: https://doi.org/10.5395/JKACD.2011.36.3.188
Published online: May 31, 2011

Department of Conservative Dentistry, Chosun University School of Dentistry, Gwangju, Korea.

Correspondence to Jeong-Bum Min, DDS, PhD. Professor, Department of Conservative Dentistry, Chosun University School of Dentistry, Gwangju, Korea. TEL, +82-62-220-3840; FAX, +82-62-223-9064; minjb@chosun.ac.kr
• Received: March 6, 2011   • Revised: April 29, 2011   • Accepted: April 29, 2011

Copyright © 2011 Korean Academy of Conservative Dentistry

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  • Objectives
    The purpose of this study was to evaluate the polymerization shrinkage stress among conventional methacrylate-based composite resins and a silorane-based composite resin.
  • Materials and Methods
    The strain gauge method was used for the determination of polymerization shrinkage strain. Specimens were divided by 3 groups according to various composite materials. Filtek Z-250 (3M ESPE) and Filtek P-60 (3M ESPE) were used as a conventional methacrylate-based composites and Filtek P-90 (3M ESPE) was used as a silorane-based composites. Measurements were recorded at each 1 second for the total of 800 seconds including the periods of light application. The results of polymerization shrinkage stress were statistically analyzed using One way ANOVA and Tukey test (p = 0.05).
  • Results
    The polymerization shrinkage stress of a silorane-based composite resin was lower than those of conventional methacrylate-based composite resins (p < 0.05). The shrinkage stress between methacrylate-based composite resin groups did not show significant difference (p > 0.05).
  • Conclusions
    Within the limitation of this study, silorane-based composites showed lower polymerization shrinkage stress than methacrylate-based composites. We need to investigate more into polymerization shrinkage stress with regard to elastic modulus of silorane-based composites for the precise result.
  • Keywords: Methacrylate composite; Polymerization shrinkage stress; Silorane composite; Strain gauge
Figure 1
Structure of strain gauge.
jkacd-36-188-g001.jpg
Figure 2
Schematic diagram of specimen and preparation.
jkacd-36-188-g002.jpg
Figure 3
Analysis of stress in a thick-walled acrylic ring.
jkacd-36-188-g003.jpg
Figure 4
Change of shrinkage stress (MPa) in each group for 800 seconds.
jkacd-36-188-g004.jpg
Table 1
Composites used in the study
jkacd-36-188-i001.jpg
Table 2
Values of shrinkage stress in each group at each measuring time (MPa)

Mean ± SD, Different letters indicate significant difference between groups (p < 0.05).

SD, Standard deviation.

jkacd-36-188-i002.jpg
  • 1. Kwon YC, Lee IB. Polymerization shringage of kinetics of silorane-based composites. J Korean Acad Conserv Dent. 2010;35: 51-58.Article
  • 2. Peutzfeldt A. Resin composites in dentistry: the monomer systems. Eur J Oral Sci. 1997;105: 97-116.ArticlePubMed
  • 3. Braga RR, Ferracane FL. Alternatives in polymerization contraction stress management. Crit Rev Oral Biol Med. 2004;15: 176-184.ArticlePubMed
  • 4. Davidson CL, Feilzer AJ. Polymerization shrinkage and polymerization shrinkage stress in polymer-based restoratives. J Dent. 1997;25: 435-440.ArticlePubMed
  • 5. Kleverlaan CJ, Feilzer AJ. Polymerization shrinkage and contraction stress of dental resin composites. Dent Mater. 2005;21: 1150-1157.ArticlePubMed
  • 6. Song YX, Inoue K. Linear shrinkage of photo-activated composite resins during setting. J Oral Rehabil. 2001;28: 335-341.ArticlePubMed
  • 7. Lee IB, Cho BH, Son HH, Um CM. A new method to measure the polymerization shrinkage kinetics of light cured composites. J Oral Rehabil. 2005;32: 304-314.ArticlePubMed
  • 8. Dauvillier BS, Aarnts MP, Feilzer AJ. Developments in shrinkage control of adhesive restoratives. J Esthet Dent. 2000;12: 291-299.ArticlePubMed
  • 9. Carvalho RM, Pereira JC, Yoshiyama M, Pashley DH. A review of polymerization contraction: the influence of stress development versus stress relief. Oper Dent. 1996;21: 17-24.PubMed
  • 10. Park J, Chang J, Ferracane J, Lee IB. How should composite be layered to reduce shrinkage stress: incremental or bulk filling? Dent Mater. 2008;24: 1501-1505.ArticlePubMed
  • 11. Lee MR, Cho BH, Son HH, Um CM, Lee IB. Influence of cavity dimension and restoration methods on the cusp deflection of premolars in composite restoration. Dent Mater. 2007;23: 288-295.ArticlePubMed
  • 12. Weinmann W, Thalacker C, Guggenberg R. Siloranes in dental composites. Dent Mater. 2005;21: 68-74.ArticlePubMed
  • 13. Stansbury JW, Trujillo-Lemon M, Lu H, Ding X, Lin Y, Ge J. Conversion-dependent shrinkage stress and strain in dental resins and composites. Dent Mater. 2005;21: 56-67.ArticlePubMed
  • 14. Papadogiannis D, Kakaboura A, Palaghias G, Eliades G. Setting characteristics and cavity adaptation of low-shrinking resin composites. Dent Mater. 2009;25: 1509-1516.ArticlePubMed
  • 15. Miletic V, Ivanovic V, Dzeletovic B, Lezaja M. Temperature changes in Silorane-, Ormocer-, and Dimethacrylate-based composites and pulp chamber roof during light-curing. J Esthet Restor Dent. 2009;21: 122-132.ArticlePubMed
  • 16. Palin WM, Fleming GJP, Nathwani H, Burke FJT, Randall RC. in vitro cuspal deflection and microleakage of maxillary premolars restored with novel low-hrink dental composites. Dent Mater. 2005;21: 324-335.PubMed
  • 17. Sakaguchi RL, Sasik CT, Bunczak MA. Strain gauge method for measuring polymerization contraction of composite restoratives. J Dent. 1991;19: 312-316.PubMed
  • 18. Sakaguchi RL, Douglas WH. Strain gauge measurement of polymerization shrinkage. J Dent Res. 1989;68: 977.
  • 19. Sakaguchi RL, Douglas WH, Peters MC. Curing light performance and polymerization fo composite restorative materials. J Dent. 1992;20: 183-188.PubMed
  • 20. Lindeburg MR. Civil engineering reference manual. 1989;5th ed. Belmont, CA: Professional; 12-27.
  • 21. Peutzfeldt A. Resin composites in dentistry: the monomer systems. Eur J Oral Sci. 1997;105: 97-116.ArticlePubMed
  • 22. Chappelow CC, Pinzino CS, Power MD, Eick JD. Photocured epoxy/SOC matrix resin systems for dental composites. Polymer Reprints. 1997;38: 90-91.
  • 23. Cadenaro M, Biasotto M, Scuor N, Breschi L, Davidson CL, Lenarda R. Assessment of polymerization contraction stress of three composite resins. Dent Mater. 2008;24: 681-685.ArticlePubMed
  • 24. Braga RR, Hilton TJ, Ferracane JL. Contraction stress of flowable composite materials and their efficacy as stress-relieving layers. J Am Dent Assoc. 2003;134: 721-728.ArticlePubMed
  • 25. Seo DG, Min SH, Lee IB. Effect of instrument compliance on the polymerization shrinkage stress measurements of dental resin composites. J Korean Acad Conserv Dent. 2009;34: 145-153.Article
  • 26. Boaro LC, Gonçalves F, Guimarães TC, Ferracane JL, Versluis A, Braga RR. Polymerization stress, shrinkage and elastic modulus of current low-shrinkage restorative composites. Dent Mater. 2010;26: 1144-1150.PubMed
  • 27. Condon JR, Ferracane JL. Assessing the effect of composite formulation on polymerization stress. J Am Dent Assoc. 2000;131: 497-503.ArticlePubMed
  • 28. Watts DC, Vogel K, Marouf AS. Shrinkage stress reduction in resin-composites of increasing particle concentration. J Dent Res. 2002;81(Special Issue A):308. Abstract #2444.PubMed
  • 29. Obici AC, Sinhoreti MAC, de Goes MF, Consai S, Sobrinho LC. Effect of the photo-activation method on polymerization shrinkage of restorative composites. Oper Dent. 2002;27: 192-198.PubMed
  • 30. Ferracane JL. Developing a more complete understanding of stresses produced in dental composites during polymerization. Dent Mater. 2005;21: 36-42.PubMed

Tables & Figures

Figure 1
Structure of strain gauge.
jkacd-36-188-g001.jpg
Figure 2
Schematic diagram of specimen and preparation.
jkacd-36-188-g002.jpg
Figure 3
Analysis of stress in a thick-walled acrylic ring.
jkacd-36-188-g003.jpg
Figure 4
Change of shrinkage stress (MPa) in each group for 800 seconds.
jkacd-36-188-g004.jpg
Table 1
Composites used in the study
jkacd-36-188-i001.jpg
Table 2
Values of shrinkage stress in each group at each measuring time (MPa)

Mean ± SD, Different letters indicate significant difference between groups (p < 0.05).

SD, Standard deviation.

jkacd-36-188-i002.jpg

REFERENCES

  • 1. Kwon YC, Lee IB. Polymerization shringage of kinetics of silorane-based composites. J Korean Acad Conserv Dent. 2010;35: 51-58.Article
  • 2. Peutzfeldt A. Resin composites in dentistry: the monomer systems. Eur J Oral Sci. 1997;105: 97-116.ArticlePubMed
  • 3. Braga RR, Ferracane FL. Alternatives in polymerization contraction stress management. Crit Rev Oral Biol Med. 2004;15: 176-184.ArticlePubMed
  • 4. Davidson CL, Feilzer AJ. Polymerization shrinkage and polymerization shrinkage stress in polymer-based restoratives. J Dent. 1997;25: 435-440.ArticlePubMed
  • 5. Kleverlaan CJ, Feilzer AJ. Polymerization shrinkage and contraction stress of dental resin composites. Dent Mater. 2005;21: 1150-1157.ArticlePubMed
  • 6. Song YX, Inoue K. Linear shrinkage of photo-activated composite resins during setting. J Oral Rehabil. 2001;28: 335-341.ArticlePubMed
  • 7. Lee IB, Cho BH, Son HH, Um CM. A new method to measure the polymerization shrinkage kinetics of light cured composites. J Oral Rehabil. 2005;32: 304-314.ArticlePubMed
  • 8. Dauvillier BS, Aarnts MP, Feilzer AJ. Developments in shrinkage control of adhesive restoratives. J Esthet Dent. 2000;12: 291-299.ArticlePubMed
  • 9. Carvalho RM, Pereira JC, Yoshiyama M, Pashley DH. A review of polymerization contraction: the influence of stress development versus stress relief. Oper Dent. 1996;21: 17-24.PubMed
  • 10. Park J, Chang J, Ferracane J, Lee IB. How should composite be layered to reduce shrinkage stress: incremental or bulk filling? Dent Mater. 2008;24: 1501-1505.ArticlePubMed
  • 11. Lee MR, Cho BH, Son HH, Um CM, Lee IB. Influence of cavity dimension and restoration methods on the cusp deflection of premolars in composite restoration. Dent Mater. 2007;23: 288-295.ArticlePubMed
  • 12. Weinmann W, Thalacker C, Guggenberg R. Siloranes in dental composites. Dent Mater. 2005;21: 68-74.ArticlePubMed
  • 13. Stansbury JW, Trujillo-Lemon M, Lu H, Ding X, Lin Y, Ge J. Conversion-dependent shrinkage stress and strain in dental resins and composites. Dent Mater. 2005;21: 56-67.ArticlePubMed
  • 14. Papadogiannis D, Kakaboura A, Palaghias G, Eliades G. Setting characteristics and cavity adaptation of low-shrinking resin composites. Dent Mater. 2009;25: 1509-1516.ArticlePubMed
  • 15. Miletic V, Ivanovic V, Dzeletovic B, Lezaja M. Temperature changes in Silorane-, Ormocer-, and Dimethacrylate-based composites and pulp chamber roof during light-curing. J Esthet Restor Dent. 2009;21: 122-132.ArticlePubMed
  • 16. Palin WM, Fleming GJP, Nathwani H, Burke FJT, Randall RC. in vitro cuspal deflection and microleakage of maxillary premolars restored with novel low-hrink dental composites. Dent Mater. 2005;21: 324-335.PubMed
  • 17. Sakaguchi RL, Sasik CT, Bunczak MA. Strain gauge method for measuring polymerization contraction of composite restoratives. J Dent. 1991;19: 312-316.PubMed
  • 18. Sakaguchi RL, Douglas WH. Strain gauge measurement of polymerization shrinkage. J Dent Res. 1989;68: 977.
  • 19. Sakaguchi RL, Douglas WH, Peters MC. Curing light performance and polymerization fo composite restorative materials. J Dent. 1992;20: 183-188.PubMed
  • 20. Lindeburg MR. Civil engineering reference manual. 1989;5th ed. Belmont, CA: Professional; 12-27.
  • 21. Peutzfeldt A. Resin composites in dentistry: the monomer systems. Eur J Oral Sci. 1997;105: 97-116.ArticlePubMed
  • 22. Chappelow CC, Pinzino CS, Power MD, Eick JD. Photocured epoxy/SOC matrix resin systems for dental composites. Polymer Reprints. 1997;38: 90-91.
  • 23. Cadenaro M, Biasotto M, Scuor N, Breschi L, Davidson CL, Lenarda R. Assessment of polymerization contraction stress of three composite resins. Dent Mater. 2008;24: 681-685.ArticlePubMed
  • 24. Braga RR, Hilton TJ, Ferracane JL. Contraction stress of flowable composite materials and their efficacy as stress-relieving layers. J Am Dent Assoc. 2003;134: 721-728.ArticlePubMed
  • 25. Seo DG, Min SH, Lee IB. Effect of instrument compliance on the polymerization shrinkage stress measurements of dental resin composites. J Korean Acad Conserv Dent. 2009;34: 145-153.Article
  • 26. Boaro LC, Gonçalves F, Guimarães TC, Ferracane JL, Versluis A, Braga RR. Polymerization stress, shrinkage and elastic modulus of current low-shrinkage restorative composites. Dent Mater. 2010;26: 1144-1150.PubMed
  • 27. Condon JR, Ferracane JL. Assessing the effect of composite formulation on polymerization stress. J Am Dent Assoc. 2000;131: 497-503.ArticlePubMed
  • 28. Watts DC, Vogel K, Marouf AS. Shrinkage stress reduction in resin-composites of increasing particle concentration. J Dent Res. 2002;81(Special Issue A):308. Abstract #2444.PubMed
  • 29. Obici AC, Sinhoreti MAC, de Goes MF, Consai S, Sobrinho LC. Effect of the photo-activation method on polymerization shrinkage of restorative composites. Oper Dent. 2002;27: 192-198.PubMed
  • 30. Ferracane JL. Developing a more complete understanding of stresses produced in dental composites during polymerization. Dent Mater. 2005;21: 36-42.PubMed

Citations

Citations to this article as recorded by  
  • Polymerization shrinkage and stress analysis during dental restoration observed by digital image correlation method
    Jung-Hoon Park, Nak-Sam Choi
    Journal of Mechanical Science and Technology.2021; 35(12): 5435.     CrossRef
  • Evaluation of the color stability of light cured composite resins according to the resin matrices
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    Korean Journal of Dental Materials.2019; 46(2): 109.     CrossRef
  • Behavior of Polymerization Shrinkage Stress of Methacrylate-based Composite and Silorane-based Composite during Dental Restoration
    Jung-Hoon Park, Nak-Sam Choi
    Composites Research.2015; 28(1): 6.     CrossRef
  • Microtensile bond strength of silorane-based composite specific adhesive system using different bonding strategies
    Laura Alves Bastos, Ana Beatriz Silva Sousa, Brahim Drubi-Filho, Fernanda de Carvalho Panzeri Pires-de-Souza, Lucas da Fonseca Roberti Garcia
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    Evaluation of polymerization shrinkage stress in silorane-based composites
    J Korean Acad Conserv Dent. 2011;36(3):188-195.   Published online May 31, 2011
    DOI: https://doi.org/10.5395/JKACD.2011.36.3.188
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Evaluation of polymerization shrinkage stress in silorane-based composites
Image Image Image Image
Figure 1 Structure of strain gauge.
Figure 2 Schematic diagram of specimen and preparation.
Figure 3 Analysis of stress in a thick-walled acrylic ring.
Figure 4 Change of shrinkage stress (MPa) in each group for 800 seconds.

Figure 1

Figure 2

Figure 3

Figure 4

Evaluation of polymerization shrinkage stress in silorane-based composites

Composites used in the study

Values of shrinkage stress in each group at each measuring time (MPa)

Mean ± SD, Different letters indicate significant difference between groups (p < 0.05).

SD, Standard deviation.
Table 1 Composites used in the study

Table 2 Values of shrinkage stress in each group at each measuring time (MPa)

Mean ± SD, Different letters indicate significant difference between groups (p < 0.05).

SD, Standard deviation.

Table 1

Table 2

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