Restorative Dentistry & Endodontics

Research Articles

Microleakage and characteristics of resin-tooth tissues interface of a self-etch and an etch-and-rinse adhesive systems: Xuan Vinh Tran, Khanh Quang Tran; Restor Dent Endod 2021;46(2):e30. Published online May 18, 2021; DOI: https://doi.org/10.5395/rde.2021.46.e30

Objectives

This study was conducted to compare the microleakage and characteristics of the resin-tooth tissue interface between self-etch and etch-and-rinse adhesive systems after 48 hours and 3 months.

Materials and Methods

40 extracted premolar teeth were randomly divided into 2 groups: 1-step self-etch adhesive system – Optibond™ All-In-One, and 2-step etch-and-rinse adhesive system - Adper™ Single Bond 2. Both groups were subjected to 500 thermocycles (5°C–55°C) before scanning electron microscope (SEM) analysis or microleakage trial at 48-hour and 3-month time periods.

Results

SEM images showed the hybrid layer thickness, diameter, and length of resin tags of the self-etch adhesive (0.42 ± 0.14 µm; 1.49 ± 0.45 µm; 16.35 ± 14.26 µm) were smaller than those of the etch-and-rinse adhesive (4.39 ± 1.52 µm; 3.49 ± 1 µm; 52.81 ± 35.81 µm). In dentin, the microleakage scores of the 2 adhesives were not different in both time periods (48 hours/3 months). However, the microleakage score of etch-and-rinse adhesive increased significantly after 3 months (0.8 ± 0.63 and 1.9 ± 0.88, p < 0.05).

Conclusions

The self-etch adhesive exhibited better long-term sealing ability in dentin when compared to that of the etch-and-rinse adhesive. The greater hybrid layer thickness and dimensions of resin tags did not guarantee reliable, long-lasting sealing in the bonding area.

Citations

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Efficacy of different adhesive systems in bonding direct resin composite restorations: a systematic review and meta-analysis
Ravinder S. Saini, Rajesh Vyas, Sunil Kumar Vaddamanu, Syed Altafuddin Quadri, Seyed Ali Mosaddad, Artak Heboyan
Evidence-Based Dentistry.2025;[Epub] CrossRef
Resin tags formation by modified Renewal MI formulations in a carious dentine model
Nabih Alkhouri, Wendy Xia, Paul Ashley, Anne Young
Frontiers in Oral Health.2024;[Epub] CrossRef
Effect of propolis added to single‐bottle adhesives on water permeation through the hybrid layer
Lucineide Silva da Rocha, Daniela Ferreira de Oliveira, Cinthya Luna Veloso de Lima, Ticiano Gomes do Nascimento, Johnnatan Duarte de Freitas, Jeniffer Mclaine Duarte de Freitas, Isabel Cristina Celerino de Moraes Porto
European Journal of Oral Sciences.2024;[Epub] CrossRef
Exploration and preliminary clinical investigation of an adhesive approach for primary tooth restoration
Xiangqin Xu, Jiansheng Zhu, May Lei Mei, Huaying Wu, Kaipeng Xie, Shoulin Wang, Yaming Chen
The Journal of Biomedical Research.2023; 37(2): 138. CrossRef
Adhesion to enamel and dentine: an update
Rana Alkattan
Primary Dental Journal.2023; 12(3): 33. CrossRef
Effects of carbodiimide combined with ethanol–wet bonding pretreatment on dentin bonding properties: an in vitro study
Xiaoxiao You, Long Chen, Jie Xu, Sihui Li, Zhenghao Zhang, Ling Guo
PeerJ.2022; 10: e14238. CrossRef
The effects of amalgam contamination and different surface modifications on microleakage of dentin bonded to bulk fill composite when using different adhesive protocols
Nojoud Alshehri, Abdullah Aljamhan, Mohammed Bin-Shuwaish
BMC Oral Health.2022;[Epub] CrossRef
Development of low-shrinkage dental adhesives via blending with spiroorthocarbonate expanding monomer and unsaturated epoxy resin monomer
Zonghua Wang, Xiaoran Zhang, Shuo Yao, Jiaxin Zhao, Chuanjian Zhou, Junling Wu
Journal of the Mechanical Behavior of Biomedical Materials.2022; 133: 105308. CrossRef
Influence of silver nanoparticles on the resin-dentin bond strength and antibacterial activity of a self-etch adhesive system
Jia Wang, Wei Jiang, Jingping Liang, Shujun Ran
The Journal of Prosthetic Dentistry.2022; 128(6): 1363.e1. CrossRef

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Effect of smear layer deproteinization on bonding of self-etch adhesives to dentin: a systematic review and meta-analysis: Khaldoan H. Alshaikh, Hamdi H. H. Hamama, Salah H. Mahmoud; Restor Dent Endod 2018;43(2):e14. Published online March 6, 2018; DOI: https://doi.org/10.5395/rde.2018.43.e14

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Objectives

The aim of this systematic review was to critically analyze previously published studies of the effects of dentin surface pretreatment with deproteinizing agents on the bonding of self-etch (SE) adhesives to dentin. Additionally, a meta-analysis was conducted to quantify the effects of the above-mentioned surface pretreatment methods on the bonding of SE adhesives to dentin.

Materials and Methods

An electronic search was performed using the following databases: Scopus, PubMed and ScienceDirect. The online search was performed using the following keywords: ‘dentin’ or ‘hypochlorous acid’ or ‘sodium hypochlorite’ and ‘self-etch adhesive.’ The following categories were excluded during the assessment process: non-English articles, randomized clinical trials, case reports, animal studies, and review articles. The reviewed studies were subjected to meta-analysis to quantify the effect of the application time and concentration of sodium hypochlorite (NaOCl) and hypochlorous acid (HOCl) deproteinizing agents on bonding to dentin.

Results

Only 9 laboratory studies fit the inclusion criteria of this systematic review. The results of the meta-analysis revealed that the pooled average microtensile bond strength values to dentin pre-treated with deproteinizing agents (15.71 MPa) was significantly lower than those of the non-treated control group (20.94 MPa).

Conclusions

In light of the currently available scientific evidence, dentin surface pretreatment with deproteinizing agents does not enhance the bonding of SE adhesives to dentin. The HOCl deproteinizing agent exhibited minimal adverse effects on bonding to dentin in comparison with NaOCl solutions.

Citations

Citations to this article as recorded by

Evaluating the remnants of Al 2 O 3 particles on different dentine substrate after sandblasting and various cleaning protocols
Faeze Hamze, Khotan Aflatoonian, Mahshid Mohammadibassir, Mohammad-Bagher Rezvani
Journal of Adhesion Science and Technology.2025; 39(6): 869. CrossRef
Preservation Strategies for Interfacial Integrity in Restorative Dentistry: A Non-Comprehensive Literature Review
Carmem S. Pfeifer, Fernanda S. Lucena, Fernanda M. Tsuzuki
Journal of Functional Biomaterials.2025; 16(2): 42. CrossRef
Outcome of Er, Cr:YSGG laser and antioxidant pretreatments on bonding quality to caries-induced dentin
Lamiaa M. Moharam, Haidy N. Salem, Ahmed Abdou, Rasha H. Afifi
BMC Oral Health.2025;[Epub] CrossRef
A comparison of different cleaning approaches for blood contamination after curing universal adhesives on the dentine surface
Ting Liu, Haifeng Xie, Chen Chen
Dental Materials.2024; 40(11): 1786. CrossRef
Effect of fiber-reinforced direct restorative materials on the fracture resistance of endodontically treated mandibular molars restored with a conservative endodontic cavity design
Merve Nezir, Beyza Arslandaş Dinçtürk, Ceyda Sarı, Cemile Kedici Alp, Hanife Altınışık
Clinical Oral Investigations.2024;[Epub] CrossRef
Effect of the use of bromelain associated with bioactive glass-ceramic on dentin/adhesive interface
Rocio Geng Vivanco, Ana Beatriz Silva Sousa, Viviane de de Cássia Oliveira, Mário Alexandre Coelho Sinhoreti, Fernanda de Carvalho Panzeri Pires-de-Souza
Clinical Oral Investigations.2024;[Epub] CrossRef
Experimental and Chitosan-Infused Adhesive with Dentin Pretreated with Femtosecond Laser, Methylene Blue-Activated Low-Level Laser, and Phosphoric Acid
Fahad Alkhudhairy
Photobiomodulation, Photomedicine, and Laser Surgery.2024; 42(10): 634. CrossRef
Evaluation of Effective Bond Strength of Composite Resin to Etched Dentin after Dentin Pretreatment: An In-vitro Study
Muhammed Bilal, Shiraz Pasha, Arathi S. Nair
Journal of the Scientific Society.2024; 51(4): 545. CrossRef
Comparison of Different Dentin Deproteinizing Agents on Bond Strength and Microleakage of Universal Adhesive to Dentin
Fatih Bedir, Gül Yıldız Telatar
Journal of Advanced Oral Research.2023; 14(1): 44. CrossRef
Addition of metal chlorides to a HOCl conditioner can enhance bond strength to smear layer deproteinized dentin
Kittisak Sanon, Antonin Tichy, Takashi Hatayama, Ornnicha Thanatvarakorn, Taweesak Prasansuttiporn, Takahiro Wada, Yasushi Shimada, Keiichi Hosaka, Masatoshi Nakajima
Dental Materials.2022; 38(8): 1235. CrossRef
Internal and Marginal Adaptation of Adhesive Resin Cements Used for Luting Inlay Restorations: An In Vitro Micro-CT Study
Linah M. Ashy, Hanadi Marghalani
Materials.2022; 15(17): 6161. CrossRef
Collagen-depletion strategies in dentin as alternatives to the hybrid layer concept and their effect on bond strength: a systematic review
António H. S. Delgado, Madalena Belmar Da Costa, Mário Cruz Polido, Ana Mano Azul, Salvatore Sauro
Scientific Reports.2022;[Epub] CrossRef
NaOCl Application after Acid Etching and Retention of Cervical Restorations: A 3-Year Randomized Clinical Trial
M Favetti, T Schroeder, AF Montagner, RR Moraes, T Pereira-Cenci, MS Cenci
Operative Dentistry.2022; 47(3): 268. CrossRef
Resin infiltrant protects deproteinized dentin against erosive and abrasive wear
Ana Theresa Queiroz de Albuquerque, Bruna Oliveira Bezerra, Isabelly de Carvalho Leal, Maria Denise Rodrigues de Moraes, Mary Anne S. Melo, Vanara Florêncio Passos
Restorative Dentistry & Endodontics.2022;[Epub] CrossRef
Bis[2-(Methacryloyloxy) Ethyl] Phosphate as a Primer for Enamel and Dentine
R. Alkattan, G. Koller, S. Banerji, S. Deb
Journal of Dental Research.2021; 100(10): 1081. CrossRef
Influence of Dentine Pre-Treatment by Sandblasting with Aluminum Oxide in Adhesive Restorations. An In Vitro Study
Bruna Sinjari, Manlio Santilli, Gianmaria D’Addazio, Imena Rexhepi, Alessia Gigante, Sergio Caputi, Tonino Traini
Materials.2020; 13(13): 3026. CrossRef
A novel prime-&-rinse mode using MDP and MMPs inhibitors improves the dentin bond durability of self-etch adhesive
Jingqiu Xu, Mingxing Li, Wenting Wang, Zhifang Wu, Chaoyang Wang, Xiaoting Jin, Ling Zhang, Wenxiang Jiang, Baiping Fu
Journal of the Mechanical Behavior of Biomedical Materials.2020; 104: 103698. CrossRef
The effects of deproteinization and primer treatment on microtensile bond strength of self-adhesive resin cement to dentin
In-Hye Bae, Sung-Ae Son, Jeong-Kil Park
Korean Journal of Dental Materials.2019; 46(2): 99. CrossRef
Effect of Papain and Bromelain Enzymes on Shear Bond Strength of Composite to Superficial Dentin in Different Adhesive Systems
Farahnaz Sharafeddin, Mina Safari
The Journal of Contemporary Dental Practice.2019; 20(9): 1077. CrossRef

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Comparing the effect of a desensitizing material and a self-etch adhesive on dentin sensitivity after periodontal surgery: a randomized clinical trial: Hila Hajizadeh, Atefeh Nemati-Karimooy, Sara Majidinia, Amir Moeintaghavi, Marjaneh Ghavamnasiri; Restor Dent Endod 2017;42(3):168-175. Published online July 21, 2017; DOI: https://doi.org/10.5395/rde.2017.42.3.168

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Objectives

This double-blind randomized placebo-controlled clinical trial evaluated the ability of a desensitizing agent and a self-etch adhesive on cervical dentin sensitivity (CDS) after periodontal surgery.

Materials and Methods

Ninety hypersensitive teeth of 13 subjects were included in the study. After periodontal surgery, the teeth of each posterior sextant treated with one of the following materials: G1: Clearfil S³ Bond (Kuraray Dental), G2: Gluma Desensitizer (Heraeus Kulzer), and G3: placebo (water). The sensitivity was assessed using evaporative stimuli before treatment (baseline, T0), 1 day after treatment (T1), after 1 week (T2), and after 1 month (T3) according to visual analog scale (VAS).

Results

Following the treatment, all the 3 groups showed significant reduction of CDS in T1 compared to T0. Reduction of CDS between T1 and T2 was observed only in G1 but there was no significant difference between T2 and T3 in this group. Although we observed a significant difference in T3 compared to T1 and T2 in G2 and G3, comparison of treatment groups in each assessment time showed a significant difference only in T3. According to paired comparison, this was due to the difference between G2 and G3.

Conclusions

Dentin sensitivity following periodontal surgery will decrease spontaneously over time, but treating the sensitive teeth with Gluma Desensitizer and Clearfil S³ Bond can have some benefits.

Citations

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Biomineralization reaction from nanosized calcium silicate: A new method for reducing dentin hypersensitivity
Mi-Jeong Jeon, Yu-Sung Choi, Jeong-Kil Park, Jin-Soo Ahn, Yu-Chih Chiang, Deog-Gyu Seo
Journal of Dental Sciences.2025; 20(1): 428. CrossRef
Efficacy of seventh generation bonding agents as desensitizers in patients with dentin hypersensitivity: a randomized clinical trial
Sumaiya Shabbir, Shahbaz Ahmed, Syed Jaffar Abbas Zaidi, Sania Riaz, Huma Sarwar, Muhammad Taqi, Zia ur Rahman Khan
BMC Oral Health.2024;[Epub] CrossRef
Investigation of the crystal formation from calcium silicate in human dentinal tubules and the effect of phosphate buffer saline concentration
Mi-Jeong Jeon, Jin-Soo Ahn, Jeong-Kil Park, Deog-Gyu Seo
Journal of Dental Sciences.2024; 19(4): 2278. CrossRef
The effect of fluoride iontophoresis on seal ability of self-etch adhesive in human dentin in vitro
Kanittha Kijsamanmith, Parintorn Wallanon, Chanya Pitchayasatit, Poonnapha Kittiratanaviwat
BMC Oral Health.2022;[Epub] CrossRef
The study of toothpaste desensitizing properties
S. B. Ulitovskiy, O. V. Kalinina, A. A. Leontev, O. V. Khabarova, L. I. Pankrateva, E. S. Soloveva, N. K. Fok
Parodontologiya.2022; 27(1): 81. CrossRef
Effectiveness and cytotoxicity of two desensitizing agents: a dentin permeability measurement and dentin barrier testing in vitro study
Ruodan Jiang, Yongxiang Xu, Feilong Wang, Hong Lin
BMC Oral Health.2022;[Epub] CrossRef
A randomized clinical trial of dentin hypersensitivity reduction over one month after a single topical application of comparable materials
Samar Hatem Abuzinadah, Abdulrahman Jafar Alhaddad
Scientific Reports.2021;[Epub] CrossRef
Comparison between effectiveness of dentine desensitizer and one bottle self-etch adhesive on dentine hypersensitivity
Muhammad Zohaib Younus, Muhammad Adeel Ahmed, Azeem Ul Yaqin Syed, Jiand Malik Baloch, Muhammad Ali, Abubakar Sheikh
Technology and Health Care.2021; 29(6): 1153. CrossRef
A long-term evaluation of experimental potassium oxalate concentrations on dentin hypersensitivity reduction: A triple-blind randomized clinical trial
Alexia da Mata Galvão, Livia Fávaro Zeola, Guilherme Faria Moura, Daniela Navarro Ribeiro Teixeira, Ramon Corrêa de Queiroz Gonzaga, Gisele Rodrigues da Silva, Paulo Vinícius Soares
Journal of Dentistry.2019; 89: 103180. CrossRef

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Effects of endodontic tri-antibiotic paste on bond strengths of dentin adhesives to coronal dentin: Parvin Mirzakoucheki, Ricardo Walter, Navid Khalighinejad, Maryam Zare Jahromi, Sanaz Mirsattari, Navid Akbarzadeh; Restor Dent Endod 2015;40(2):136-142. Published online February 12, 2015; DOI: https://doi.org/10.5395/rde.2015.40.2.136

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Objectives

The aim of this study was to evaluate the effects of tri-antibiotic paste (TAP) on microtensile bond strengths (MTBS) of dental adhesives to dentin.

Materials and Methods

Sixty extracted molars had their occlusal surfaces flattened to expose dentin. They were divided into two groups, i.e., control group with no dentin treatment and experimental group with dentin treatment with TAP. After 10 days, specimens were bonded using self-etch (Filtek P90 adhesive) or etch-and-rinse (Adper Single Bond Plus) adhesives and restored with composite resin. Teeth were sectioned into beams, and the specimens were subjected to MTBS test. Data were analyzed using two-way ANOVA and post hoc Tukey tests.

Results

There was a statistically significant interaction between dentin treatment and adhesive on MTBS to coronal dentin (p = 0.003). Despite a trend towards worse MTBS being noticed in the experimental groups, TAP application showed no significant effect on MTBS (p = 0.064).

Conclusions

The etch-and-rinse adhesive Adper Single Bond Plus presented higher mean bond strengths than the self-etch adhesive Filtek P90, irrespective of the group. The superior bond performance for Adper Single Bond when compared to Filtek P90 adhesive was confirmed by a fewer number of adhesive failures. The influence of TAP in bond strength is insignificant.

Citations

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Efecto antimicrobiano como medicación intraconducto de la pasta triantibiótica.
Paúl Sebastián Ulloa Amores, Diana Álvarez Álvarez, María Elizabeth Moscoso Abad, Magda Zulay Bastidas Calva
Revista de la Asociación Dental Mexicana.2024; 81(4): 211. CrossRef
Effect of Intracanal Medicaments on Push-out Bond Strength of Calcium Silicate-based Materials
Hyuntae Jeong, Sunmi Yang, Seonmi Kim, Namki Choi, Jaehwan Kim
THE JOURNAL OF THE KOREAN ACADEMY OF PEDTATRIC DENTISTRY.2018; 45(4): 455. CrossRef

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Effect of additional etching and ethanol-wet bonding on the dentin bond strength of one-step self-etch adhesives: Joonghee Ahn, Kyoung-Hwa Jung, Sung-Ae Son, Bock Hur, Yong-Hoon Kwon, Jeong-Kil Park; Restor Dent Endod 2015;40(1):68-74. Published online November 18, 2014; DOI: https://doi.org/10.5395/rde.2015.40.1.68

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Objectives

This study examined the effects of additional acid etching on the dentin bond strength of one-step self-etch adhesives with different compositions and pH. The effect of ethanol wetting on etched dentin bond strength of self-etch adhesives was also evaluated.

Materials and Methods

Forty-two human permanent molars were classified into 21 groups according to the adhesive types (Clearfil SE Bond [SE, control]; G-aenial Bond [GB]; Xeno V [XV]; Beauti Bond [BB]; Adper Easy Bond [AE]; Single Bond Universal [SU]; All Bond Universal [AU]), and the dentin conditioning methods. Composite resins were placed on the dentin surfaces, and the teeth were sectioned. The microtensile bond strength was measured, and the failure mode of the fractured specimens was examined. The data were analyzed statistically using two-way ANOVA and Duncan's post hoc test.

Results

In GB, XV and SE (pH ≤ 2), the bond strength was decreased significantly when the dentin was etched (p < 0.05). In BB, AE and SU (pH 2.4 - 2.7), additional etching did not affect the bond strength (p > 0.05). In AU (pH = 3.2), additional etching increased the bond strength significantly (p < 0.05). When adhesives were applied to the acid etched dentin with ethanol-wet bonding, the bond strength was significantly higher than that of the no ethanol-wet bonding groups, and the incidence of cohesive failure was increased.

Conclusions

The effect of additional acid etching on the dentin bond strength was influenced by the pH of one-step self-etch adhesives. Ethanol wetting on etched dentin could create a stronger bonding performance of one-step self-etch adhesives for acid etched dentin.

Citations

Citations to this article as recorded by

Influence of Different Application Modes of a Universal Adhesive System on the Bond Strength of Bulk‐Fill Composite Resin to Enamel and Dentin in Primary Teeth
Ali Nozari, Maryam Pakniyat Jahromi, Farnaz Haji Abbas Oghli, Zahra Jowkar, Seyed Ahmadreza Hamidi
Clinical and Experimental Dental Research.2024;[Epub] CrossRef
Effect of a novel pretreatment on the microtensile bond strength of universal adhesives with dentin
Yixiang Pan, Jiajia Xu, Xue Cai, Xiaodong Li, Xiaoyan Wang
Journal of Dental Sciences.2023; 18(3): 1148. CrossRef
Microfluidic Organ-on-A-chip: A Guide to Biomaterial Choice and Fabrication
Uyen M. N. Cao, Yuli Zhang, Julie Chen, Darren Sayson, Sangeeth Pillai, Simon D. Tran
International Journal of Molecular Sciences.2023; 24(4): 3232. CrossRef
Effect of phytic acid on bond strength and interfacial integrity of universal adhesive to deep dentin
Ahmed Mostafa Attia, Ahmed Fawzy Abo-Elezz, Rehab Khalil Safy
Brazilian Dental Journal.2022; 33(5): 116. CrossRef
Microtensile Bond Strength of Total-Etch and Self-Etch Universal Adhesives Containing 10-MDP: A Systematic Review
I. Hisham Ismail, N.A. Abdul Razak, N.D. Mohd Ramzi, M.Y.P. Mohd Yusof
The Journal of Dentists.2022; 10: 12. CrossRef
Biomodification of dentin collagen by primers with crosslinking reagents using ethanol wet bonding technique
Talita Arrais Daniel Mendes, Samuel Chillavert Dias Pascoal, Marcelo Victor Sidou Lemos, Sérgio Lima Santiago, Juliano Sartori Mendonça
International Journal of Adhesion and Adhesives.2022; 119: 103254. CrossRef
Is the presence of 10-MDP associated to higher bonding performance for self-etching adhesive systems? A meta-analysis of in vitro studies
Julia Fehrenbach, Cristina Pereira Isolan, Eliseu Aldrighi Münchow
Dental Materials.2021; 37(10): 1463. CrossRef
The effect of additional chlorhexidine and/or ethanol on the bond strength of universal adhesives
Zeynep Buket Kaynar, Magrur Kazak, Nazmiye Donmez, Evrim Eliguzeloglu Dalkilic
Journal of Adhesion Science and Technology.2021; 35(4): 375. CrossRef
Evaluation of the Effect of Cold Plasma Treatment on the Microshear Bond Strength of Composite Resin Restorations to Dentin using Different Adhesive Systems and the Effect of Thermocycling
Sara Valizadeh, Elham Farhadi, Aida Moradi, Sedighe S. Hashemikamangar
The Open Dentistry Journal.2021; 15(1): 734. CrossRef
Bond Strength of Universal Adhesives to Dentin: A Systematic Review and Meta-Analysis
Louis Hardan, Rim Bourgi, Naji Kharouf, Davide Mancino, Maciej Zarow, Natalia Jakubowicz, Youssef Haikel, Carlos Enrique Cuevas-Suárez
Polymers.2021; 13(5): 814. CrossRef
Effects of simplified ethanol–wet bonding and hydrophobic coating on resin–dentin bonding properties
Xia Wang, He Li, Liang Chen, Yue Wang, Jianfei Bai, Defei Wang, Hong Liu
Journal of Adhesion Science and Technology.2021; 35(9): 913. CrossRef
Effect of dentin biomodification techniques on the stability of the bonded interface
Nida Mehmood, Rajni Nagpal, UdaiPratap Singh, Meenal Agarwal
Journal of Conservative Dentistry.2021; 24(3): 265. CrossRef
Assessment of nanohardness, elastic modulus, and nanoleakage of the adhesive interface using the ethanol-wet-bonding technique
Mauricio Yugo Souza, Jéssica Lopes Andrade, Taciana Marco Ferraz Caneppele, Eduardo Bresciani
International Journal of Adhesion and Adhesives.2020; 99: 102572. CrossRef
The improvement of biocompatibility of adhesives
Cigdem Atalayin, Huseyin Tezel, Zeynep Ergucu, Nimet Unlu, Guliz Armagan, Taner Dagci, Timur Kose
Clinical Oral Investigations.2019; 23(8): 3213. CrossRef
Comparison of the micro-tensile bond strengths of four different universal adhesives to caries-affected dentin after ER:YAG laser irradiation
Nazmiye DÖNMEZ, Ayça Sarıalioğlu GÜNGÖR, Barış KARABULUT, Şeyda Hergüner SİSO
Dental Materials Journal.2019; 38(2): 218. CrossRef
Six-month performance of restorations produced with the ethanol-wet-bonding technique: a randomized trial
Maurício Yugo de SOUZA, Ana Luiza Barbosa JUREMA, Taciana Marco Ferraz CANEPPELE, Eduardo BRESCIANI
Brazilian Oral Research.2019;[Epub] CrossRef
Influence of ethanol-wet dentin, adhesive mode of application, and aging on bond strength of universal adhesive
Mauricio Yugo de SOUZA, Rebeca DI NICOLÓ, Eduardo BRESCIANI
Brazilian Oral Research.2018;[Epub] CrossRef
Effects of light curing modes and ethanol-wet bonding on dentin bonding properties
Mu-zi Li, Jin-rui Wang, Hong Liu, Xia Wang, Kang Gan, Xiu-ju Liu, De-li Niu, Xiao-qing Song
Journal of Zhejiang University-SCIENCE B.2016; 17(9): 703. CrossRef
Effect of an Er,Cr:YSGG laser preparation on dentin bond strength of a universal adhesive
A. Rüya Yazici, Emel Karaman, Duygu Tuncer, Gizem Berk, Atilla Ertan
Journal of Adhesion Science and Technology.2016; 30(22): 2477. CrossRef
The effect of saliva decontamination procedures on dentin bond strength after universal adhesive curing
Jayang Kim, Sungok Hong, Yoorina Choi, Sujung Park
Restorative Dentistry & Endodontics.2015; 40(4): 299. CrossRef

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A study on the compatibility between one-bottle dentin adhesives and composite resins using micro-shear bond strength: Minju Song, Yooseok Shin, Jeong-Won Park, Byoung-Duck Roh; Restor Dent Endod 2015;40(1):30-36. Published online September 26, 2014; DOI: https://doi.org/10.5395/rde.2015.40.1.30

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Objectives

This study was performed to determine whether the combined use of one-bottle self-etch adhesives and composite resins from same manufacturers have better bond strengths than combinations of adhesive and resins from different manufacturers.

Materials and Methods

25 experimental micro-shear bond test groups were made from combinations of five dentin adhesives and five composite resins with extracted human molars stored in saline for 24 hr. Testing was performed using the wire-loop method and a universal testing machine. Bond strength data was statistically analyzed using two way analysis of variance (ANOVA) and Tukey's post hoc test.

Results

Two way ANOVA revealed significant differences for the factors of dentin adhesives and composite resins, and significant interaction effect (p < 0.001). All combinations with Xeno V (Dentsply De Trey) and Clearfil S³ Bond (Kuraray Dental) adhesives showed no significant differences in micro-shear bond strength, but other adhesives showed significant differences depending on the composite resin (p < 0.05). Contrary to the other adhesives, Xeno V and BondForce (Tokuyama Dental) had higher bond strengths with the same manufacturer's composite resin than other manufacturer's composite resin.

Conclusions

Not all combinations of adhesive and composite resin by same manufacturers failed to show significantly higher bond strengths than mixed manufacturer combinations.

Citations

Citations to this article as recorded by

Influence of etching mode and composite resin type on bond strength to dentin using universal adhesive system
Stefan Dačić, Milan Miljković, Aleksandar Mitić, Goran Radenković, Marija Anđelković‐Apostolović, Milica Jovanović
Microscopy Research and Technique.2021; 84(6): 1212. CrossRef
Is the presence of 10-MDP associated to higher bonding performance for self-etching adhesive systems? A meta-analysis of in vitro studies
Julia Fehrenbach, Cristina Pereira Isolan, Eliseu Aldrighi Münchow
Dental Materials.2021; 37(10): 1463. CrossRef
Dentin bond strengths of all-in-one adhesives combined with different manufacturers’ flowable resin composites
Koichi SHINKAI, Daiki YOSHII, Akira KOIDE, Masaya SUZUKI, Shiro SUZUKI
Dental Materials Journal.2021; 40(5): 1094. CrossRef
DİŞ HEKİMLİĞİNDE ADEZİV SİSTEMLER
Elmas TÜRKER, Buket AYNA
Atatürk Üniversitesi Diş Hekimliği Fakültesi Dergisi.2018;[Epub] CrossRef
Influence of EDC on Dentin-Resin Shear Bond Strength and Demineralized Dentin Thermal Properties
Lin Tang, Yi Zhang, Yuhua Liu, Yongsheng Zhou
Materials.2016; 9(11): 920. CrossRef

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Effect of different air-drying time on the microleakage of single-step self-etch adhesives: Horieh Moosavi, Maryam Forghani, Esmatsadat Managhebi; Restor Dent Endod 2013;38(2):73-78. Published online May 28, 2013; DOI: https://doi.org/10.5395/rde.2013.38.2.73

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Objectives

This study evaluated the effect of three different air-drying times on microleakage of three self-etch adhesive systems.

Materials and Methods

Class I cavities were prepared for 108 extracted sound human premolars. The teeth were divided into three main groups based on three different adhesives: Opti Bond All in One (OBAO), Clearfil S³ Bond (CSB), Bond Force (BF). Each main group divided into three subgroups regarding the air-drying time: without application of air stream, following the manufacturer's instruction, for 10 sec more than manufacturer's instruction. After completion of restorations, specimens were thermocycled and then connected to a fluid filtration system to evaluate microleakage. The data were statistically analyzed using two-way ANOVA and Tukey-test (α = 0.05).

Results

The microleakage of all adhesives decreased when the air-drying time increased from 0 sec to manufacturer's instruction (p < 0.001). The microleakage of BF reached its lowest values after increasing the drying time to 10 sec more than the manufacturer's instruction (p < 0.001). Microleakage of OBAO and CSB was significantly lower compared to BF in all three drying time (p < 0.001).

Conclusions

Increasing in air-drying time of adhesive layer in one-step self-etch adhesives caused reduction of microleakage, but the amount of this reduction may be dependent on the adhesive components of self-etch adhesives.

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Effect of chlorhexidine application on the bond strength of resin core to axial dentin in endodontic cavity: Yun-Hee Kim, Dong-Hoon Shin; Restor Dent Endod 2012;37(4):207-214. Published online November 21, 2012; DOI: https://doi.org/10.5395/rde.2012.37.4.207

Abstract PDF PubReader ePub

Objectives

This study evaluated the influence of chlorhexidine (CHX) on the microtensile bonds strength (µTBS) of resin core with two adhesive systems to dentin in endodontic cavities.

Materials and Methods

Flat dentinal surfaces in 40 molar endodontic cavities were treated with self-etch adhesive system, Contax (DMG) and total-etch adhesive system, Adper Single Bond 2 (3M ESPE) after the following surface treatments: (1) Priming only (Contax), (2) CHX for 15 sec + rinsing + priming (Contax), (3) Etching with priming (Adper Single Bond 2), (4) Etching + CHX for 15 sec + rinsing + priming (Adper Single Bond 2). Resin composite build-ups were made with LuxaCore (DMG) using a bulk method and polymerized for 40 sec. For each condition, half of specimens were submitted to µTBS after 24 hr storage and half of them were submitted to thermocycling of 10,000 cycles between 5℃ and 55℃ before testing. The data were analyzed using ANOVA and independent t-test at a significance level of 95%.

Results

CHX pre-treatment did not affect the bond strength of specimens tested at the immediate testing period, regardless of dentin surface treatments. However, after 10,000 thermocycling, all groups showed reduced bond strength. The amount of reduction was greater in groups without CHX treatments than groups with CHX treatment. These characteristics were the same in both self-etch adhesive system and total-etch adhesive system.

Conclusions

2% CHX application for 15 sec proved to alleviate the decrease of bond strength of dentin bonding systems. No significant difference was shown in µTBS between total-etching system and self-etching system.

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Basic Researchs

Effect of 2% chlorhexidine application on microtensile bond strength of resin composite to dentin using one-step self-etch adhesives: Soon-Ham Jang, Bock Hur, Hyeon-Cheol Kim, Yong-Hun Kwon, Jeong-Kil Park; J Korean Acad Conserv Dent 2010;35(6):486-491. Published online November 30, 2010; DOI: https://doi.org/10.5395/JKACD.2010.35.6.486

Abstract PDF PubReader ePub: Objectives
This study examined the effect of 2% chlorhexidine on the µTBS of a direct composite restoration using one-step self-etch adhesives on human dentin.
Materials and Methods
Twenty-four extracted permanent molars were used. The teeth were assigned randomly to six groups (n = 10), according to the adhesive system and application of chlorhexidine. With or without the application of chlorhexidine, each adhesive system was applied to the dentin surface. After the bonding procedure, light-cure composite resin buildups were produced. The restored teeth were stored in distilled water at room temperature for 24 hours, and then cut and glued to the jig of the microtensile testing machine. A tensile load was applied until the specimen failed. The failure mode was examined using an operating microscope. The data was analyzed statistically using one-way ANOVA, Student's t-test (p < 0.05) and Scheffé's test.
Results
Regardless of the application of chlorhexidine, the Clearfil S³ Bond showed the highest µTBS, followed by G-Bond and Xeno V. Adhesive failure was the main failure mode of the dentin bonding agents tested with some samples showing cohesive failure.
Conclusions
The application of 2% chlorhexidine did not affect the µTBS of the resin composite to the dentin using a one-step self-etch adhesive.

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Effect of cutting instruments on the dentin bond strength of a self-etch adhesive: Young-Gon Lee, So-Ra Moon, Young-Gon Cho; J Korean Acad Conserv Dent 2010;35(1):13-19. Published online January 31, 2010; DOI: https://doi.org/10.5395/JKACD.2010.35.1.013

Abstract PDF PubReader ePub

The purpose of this study was to compare the microshear bond strength of a self-etching primer adhesive to dentin prepared with different diamond points, carbide burs and SiC papers, and also to determine which SiC paper yield similar strength to that of dentinal surface prepared with points or burs.

Fifty-six human molar were sectioned to expose the occlusal dentinal surfaces of crowns and slabs of 1.2 mm thick were made. Dentinal surfaces were removed with three diamond points, two carbide burs, and three SiC papers. They were divided into one of eight equal groups (n = 7); Group 1: standard diamond point(TF-12), Group 2: fine diamond point (TF-12F), Group 3: extrafine diamond point (TF-12EF), Group 4: plain-cut carbide bur (no. 245), Group 5: cross-cut carbide bur (no. 557), Group 6 : P 120-grade SiC paper, Group 7: P 220-grade SiC paper, Group 8: P 800-grade SiC paper.

Clearfil SE Bond was applied on dentinal surface and Clearfil AP-X was placed on dentinal surface using Tygon tubes. After the bonded specimens were subjected to uSBS testing, the mean uSBS (n = 20 for each group) was statistically compared using one-way ANOVA and Tukey HSD test.

In conclusion, the use of extrafine diamond point is recommended for improved bonding of Clearfil SE Bond to dentin. Also the use of P 220-grade SiC paper in vitro will be yield the results closer to dentinal surface prepared with fine diamond point or carbide burs in vivo.

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Original Articles

Enamel adhesion of light- and chemical-cured composites coupled by two step self-etch adhesives: Sae-Hee Han, Eun-Soung Kim, Young-Gon Cho; J Korean Acad Conserv Dent 2007;32(3):169-179. Published online May 31, 2007; DOI: https://doi.org/10.5395/JKACD.2007.32.3.169

Abstract PDF PubReader ePub

This study was to compare the microshear bond strength (µSBS) of light- and chemically cured composites to enamel coupled with four 2-step self-etch adhesives and also to evaluate the incompatibility between 2-step self-etch adhesives and chemically cured composite resin.

Crown segments of extracted human molars were cut mesiodistally, and a 1 mm thickness of specimen was made. They were assigned to four groups by adhesives used: SE group (Clearfil SE Bond), AdheSE group (AdheSE), Tyrian group (Tyrian SPE/One-Step Plus), and Contax group (Contax). Each adhesive was applied to a cut enamel surface as per the manufacturer's instruction. Light-cured (Filtek Z250) or chemically cured composite (Luxacore Smartmix Dual) was bonded to the enamel of each specimen using a Tygon tube. After storage in distilled water for 24 hours, the bonded specimens were subjected to µSBS testing with a crosshead speed of 1 mm/minute. The mean µSBS (n=20 for each group) was statistically compared using two-way ANOVA, Tukey HSD, and t test at 95% level. Also the interface of enamel and composite was evaluated under FE-SEM.

The results of this study were as follows;

1. The µSBS of the SE Bond group to the enamel was significantly higher than that of the AdheSE group, the Tyrian group, and the Contax group in both the light-cured and the chemically cured composite resin (p < 0.05).

2. There was not a significant difference among the AdheSE group, the Tyrian group, and the Contax group in both the light-cured and the chemically cured composite resin.

3. The µSBS of the light-cured composite resin was significantly higher than that of the chemically cured composite resin when same adhesive was applied to the enamel (p < 0.05).

4. The interface of enamel and all 2-step self-etch adhesives showed close adaptation, and so the incompatibility of the chemically cured composite resin did not show.

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Effect of pre-heating on some physical properties of composite resin
Myoung Uk Jin, Sung Kyo Kim
Journal of Korean Academy of Conservative Dentistry.2009; 34(1): 30. CrossRef

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Microshear bond strength of adhesives according to the direction of enamel rods: Young-Gon Cho, Jong-Jin Kim; J Korean Acad Conserv Dent 2005;30(4):344-351. Published online July 30, 2005; DOI: https://doi.org/10.5395/JKACD.2005.30.4.344

Abstract PDF PubReader ePub

This study compared the microshear bond strength (µSBS) to end and side of enamel rod bonded by four adhesives including two total etch adhesives and two self-etch adhesives.

Crown segments of extracted human molars were cut mesiodistally. The outer buccal or lingual surface was used as specimens cutting the ends of enamel rods, and inner slabs used as specimens cutting the sides of enamel rods.

They were assigned to four groups by used adhesives: Group 1 (All-Bond 2), Group 2 (Single Bond), Group 3 (Tyrian SPE/One-Step Plus), Group 4 (Adper Prompt L-Pop). After each adhesive was applied to enamel surface, three composite cylinders were adhered to it of each specimen using Tygon tube. After storage in distilled water for 24 hours, the bonded specimens were subjected to µSBS testing with a crosshead speed of 1 mm/minute. The results of this study were as follows;

1. The µSBS of Group 2 (16.50 ± 2.31 _MPa) and Group 4 (15.83 ± 2.33 _MPa) to the end of enamel prism was significantly higher than that of Group 1 (11.93 ± 2.25 _MPa) and Group 3 (11.97 ± 2.05 _MPa) (p < 0.05).

2. The µSBS of Group 2 (13.43 ± 2.93 _MPa) to the side of enamel prism was significantly higher than that of Group 1 (8.64 ± 1.53 _MPa), Group 3 (9.69 ± 1.80 _MPa), and Group 4 (10.56 ± 1.75 _MPa) (p < 0.05).

3. The mean µSBS to the end of enamel rod was significantly higher than that to the side of enamel rod in all group (p < 0.05).

Citations

Citations to this article as recorded by

Enamel adhesion of light- and chemical-cured composites coupled by two step self-etch adhesives
Sae-Hee Han, Eun-Soung Kim, Young-Gon Cho
Journal of Korean Academy of Conservative Dentistry.2007; 32(3): 169. CrossRef

246 View
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