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• Micro-computed tomography evaluation of volumetric polymerization shrinkage and degree of conversion of composites cured by various light power outputs
  Pablo J. ATRIA, Camila S. SAMPAIO, Eduardo CÁCERES, Jessica FERNÁNDEZ, Andre F. REIS, Marcelo GIANNINI, Paulo G. COELHO, Ronaldo HIRATA
  Dental Materials Journal.2018; 37(1): 33.     CrossRef
• Effect of the irradiance distribution from light curing units on the local micro-hardness of the surface of dental resins
  Thomas Haenel, Berenika Hausnerová, Johannes Steinhaus, Richard B.T. Price, Braden Sullivan, Bernhard Moeginger
  Dental Materials.2015; 31(2): 93.     CrossRef
• 1,3-Butadiene as an Adhesion Promoter Between Composite Resin and Dental Ceramic in a Dielectric Barrier Discharge Jet
  Geum-Jun Han, Sung-No Chung, Bae-Hyeock Chun, Chang-Keun Kim, Kyu Hwan Oh, Byeong-Hoon Cho
  Plasma Chemistry and Plasma Processing.2013; 33(2): 539.     CrossRef
• Optimal combination of 3-component photoinitiation system to increase the degree of conversion of resin monomers
  Chang-Gyu Kim, Ho-Jin Moon, Dong-Hoon Shin
  Journal of Korean Academy of Conservative Dentistry.2011; 36(4): 313.     CrossRef

The purpose of this study was to evaluate the effect of pre-heating on some physical properties of composite resin.

Eighty extracted, noncarious human molars were used in the present study. Four different temperatures of composite resin were used: 4℃, 17℃, 48℃, and 56℃. The 4℃ and 17℃ values represented the refrigerator storage temperature and room temperature respectively. For 48℃ and 56℃, composite resin was heated to the temperatures. As physical properties of composite resin, shear bond strength, microhardness, and degree of conversion were measured. The data for each group were subjected to one-way ANOVAs followed by the Tukey's HSD test at 95% confidence level.

Both in enamel and dentin, among composite resin of 4℃, 17℃, 48℃, and 56℃, the pre-heated composite resin up to 56℃ revealed the highest shear bond strength, and pre-heated composite resin to the higher temperature revealed higher shear bond strength.

Microhardness value was also higher with composite resin of higher temperature.

Degree of conversion was also higher with composite resin of the higher temperature.

In this study, it seems that pre-heating composite resin up to the higher temperature may show higher shear bond strength, higher microhardness value, and higher degree of conversion. Therefore, when using composite resin in the clinic, preheating the composite resin could be recommended to have enhanced physical properties of it.

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• Evaluation of Shear Bond Strength of Lithium Disilicate Veneers Using Pre-heated Resin Composite With Two Conventional Resin Cements: An In Vitro Study
  Ghalia Akyle, Hassan Achour
  Cureus.2024;[Epub]     CrossRef
• The different effects of preheating and heat treatment on the surface microhardness of nanohybrid resin composite
  Brelian Elok Septyarini, Irfan Dwiandhono, Dian N. Agus Imam
  Dental Journal.2020; 53(1): 6.     CrossRef

The purpose of this study was to evaluate the effect of thickness, filling methods and curing methods on the polymerization of dual cured core materials by means of microhardness test.

Two dual cured core materials, MultiCore Flow (Ivoclar Vivadent AG, Schaan, Liechtenstein) and Bis-Core (Bisco Inc., Schaumburg, IL, USA) were used in this study. 2 mm (bulky filled), 4 mm (bulky filled), 6 mm (bulky and incrementally filled) and 8 mm (bulky and incrementally filled)-thickness specimens were prepared with light cure or self cure mode. After storage at 37℃ for 24 hours, the Knoop hardness values (KHN) of top and bottom surfaces were measured and the microhardness ratio of top and bottom surfaces was calculated. The data were analyzed using one-way ANOVA and Scheffe multiple comparison test, with α = 0.05.

The effect of thickness on the polymerization of dual cured composites showed material specific results. In 2, 4 and 6 mm groups, the KHN of two materials were not affected by thickness. However, in 8 mm group of MultiCore Flow, the KHN of the bottom surface was lower than those of other groups (p < 0.05). The effect of filling methods on the polymerization of dual cured composites was different by their thickness or materials. In 6 mm thickness, there was no significant difference between bulk and incremental filling groups. In 8 mm thickness, Bis-Core showed no significant difference between groups. However, in MultiCore Flow, the microhardness ratio of bulk filling group was lower than that of incremental filling group (p < 0.05). The effect of curing methods on the polymerization of dual cured composites showed material specific results. In Bis-Core, the KHN of dual cured group were higher than those of self cured group at both surfaces (p < 0.05). However, in MultiCore Flow, the results were not similar at both surfaces. At the top surface, dual cured group showed higher KHN than that of self cured group (p < 0.05). However, in the bottom surface, dual cured group showed lower value than that of self cured group (p < 0.05).

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• Effect of curing modes on micro-hardness of dual-cure resin cements
  Ki-Deok Lee, Se-Hee Park, Jin-Woo Kim, Kyung-Mo Cho
  Journal of Korean Academy of Conservative Dentistry.2011; 36(2): 132.     CrossRef

The objective of this in situ study was to evaluate the effects of whitening strip (Claren, LG Household & Health Care Ltd, 2.6% hydrogen peroxide) and gel (Opalescence, Ultradent, 10% carbamide peroxide) on microhardness of enamel in comparison with untreated control. Extracted twenty human upper incisors were disinfected, cleaned, and labial side of each incisor sectioned into 3 fragments by 2 × 2 mm size. After sectioning, labial sides of fragments were flattened and fixed to orthodontic bracket using flowable composite resin. Specimens prepared from each tooth were attached to the labial side of upper incisors of twenty volunteers one by one and treated by three different methods: (1) untreated control (2) treated with whitening strip for 14 days (3) treated with whitening gel for 14 days.

Microhardness (Microhardness tester, Zwick) of each specimen was measured at the baseline of pre-treatment, immediate after bleaching treatment, 14 days after bleaching treatment and Knoop Hardness Number was determined. Microhardness changes of experimental groups were compared.

The results show that tooth whitening strip and gel used in this study does not effect the micro-hardness of enamel during bleaching procedure.

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• Surface Damage and Bleaching Effect according to the Application Type of Home Tooth Bleaching Applicants
  Na-Yeoun Tak, Do-Seon Lim, Hee-Jung Lim, Im-Hee Jung
  Journal of Dental Hygiene Science.2020; 20(4): 252.     CrossRef
• Effect of the bleaching light on whitening efficacy
  Jong-Hyun Park, Hye-Jin Shin, Deok-Young Park, Se-Hee Park, Jin-Woo Kim, Kyung-Mo Cho
  Journal of Korean Academy of Conservative Dentistry.2009; 34(2): 95.     CrossRef

The purpose of this study was to investigate the influence of thickness on the degree of cure of dual-cured composite core.

2, 4, 6, 8 mm thickness Luxacore Dual and Luxacore Self (DMG Inc, Hamburg, Germany) core composites were cured by bulk or incremental filling with halogen curing unit or self-cure mode. The specimens were stored at 37℃ for 24 hours and the Knoop's hardness of top and bottom surfaces were measured.

The statistical analysis was performed using ANOVA and Tukey's test at p = 0.05 significance level.

In self cure mode, polymerization is not affected by the thickness. In Luxacore dual, polymerization of the bottom surface was effective in 2, 4 and 6 (incremental) mm specimens. However the 6 (bulk) and 8 (bulk, incremental) mm filling groups showed lower bottom/top hardness ratio (p < 0.05). Within the limitation of this experiment, incremental filling is better than bulk filling in case of over 4 mm depth, and bulk filling should be avoided.

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• A Study of Composite Surface Hardness When Cured Using Special Accessories with a Curing Light
  Samir Koheil
  Dental Research and Management.2020; : 11.     CrossRef
• Effect of curing modes on micro-hardness of dual-cure resin cements
  Ki-Deok Lee, Se-Hee Park, Jin-Woo Kim, Kyung-Mo Cho
  Journal of Korean Academy of Conservative Dentistry.2011; 36(2): 132.     CrossRef

The objectives of this study was to evaluate current visible light curing units regarding microhardness and microleakage. Fourty samples of composite resin(Z-250, 3M) were cured by different light curing units(Flipo, LOKKI; Credi II, 3M; XL 3000, 3M; Optilux 500,Demetron) in acrylic blocks. Microhardness was measured using a calibrated Vickers indenter on both top and bottom surfaces after 24 hours of storage in air at room temperature. Class V cavities were prepared on buccal and lingual surfaces of fourty extracted human molars. Each margin was on enamel and dentin/cementum. Composite resin(Z-250, 3M) was filled in cavities and cured by four different light curing units(Flipo, LOKKI; Credi II, 3M; XL 3000, 3M; Optilux 500, Demetron).

The results of this syudy were as follows:

Microhardness

1. Flipo showed low microhardness compared to Optilux 500, Credi II significantly in upper surface. Flipo didn't show a significant difference compared to XL 3000.

2. The microhardness resulting from curing with Flipo was lower than that of others on lower surfaces.

Microleakage

1. Dentin margin showed significantly high dye penetration rate than enamel margin in all groups(p<0.05).

2. No significant differences were found on both enamel and dentin margin regarding curing units.

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• Comparison of Surface Microhardness of the Flowable Bulk-Fill Resin and the Packable Bulk-Fill Resin according to Light Curing Time and Distance
  Hyung-Min Kim, Moon-Jin Jeong, Hee-Jung Lim, Do-Seon Lim
  Journal of Dental Hygiene Science.2023; 23(2): 123.     CrossRef

The purpose of this study was to compare the microhardness and the fluoride content of enamel and dentin around fluoride- or non fluoride-containing restorations. Forty extracted human teeth were used and prepared cervical cavities on proximal surface. Experimental teeth were divided into five groups. Group 1 : Prime & Bond NT and Z100, Group 2 : Prime & Bond NT and F2000, Group 3 : Scotchbond Multi-Purpose and Z100, Group 4 : Scothcbond Multi-purpose and F2000, Group 5 : Fuji II LC. The cavities were filled with dentin adhesives and restorative materials. After each tooth was bisected, one half was tested microhardness and the other half was analyzed the fluoride at the enamel and dentin by an EPMA-WDX device. The results were as follows:

1. There was no statistical difference among the microhardness of enamel surface in all group.

2. The microhardness at dentin of 100 µm point in Group 2 and 20 µm point in Group 4 was lower than that of normal dentin (p>0.05).

3. There was no statistical difference among the fluoride content of enamel surface in all group.

4. The fluoride content at the dentin of 30 µm point in Group 2 and 5 were higher than those at 100 µm and 200 µm point in Group 2 and normal dentin (p<0.05).

5. At the dentin of 30 µm point, Group 2 showed higher fluoride content than Group 1 and 3, and Group 5 showed higher fluoride content than other groups.

The purpose of this study is to evaluate the polymerization ability of three different light sources by microhardness test. Stainless steel molds of 1, 2, 3, 4 and 5 mm in thickness of 7 mm in diameter were prepared. The hybrid composite Z100 was packed into the hole of the mold and curing light was activated for designated time. Three different light sources, conventional halogen, light emitting diode, and plasma arc, were used for curing of composite. Two different curing times applied; one is to follow the manufacturer's recommendation and the other is to extend the curing time of LED and plasma arc for balancing the light energy with halogen. Immediately after curing, the Vickers hardness was measured at the bottom of specimen.

The results were as follows.

The composite cured with LED showed equal to higher microhardnesss than halogen.

In conclusion, this study suggested that plasma arc needs properly extended curing time.

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• Power density of light curing units through resin inlays fabricated with direct and indirect composites
  Hoon-Sang Chang, Young-Jun Lim, Jeong-Mi Kim, Sung-Ok Hong
  Journal of Korean Academy of Conservative Dentistry.2010; 35(5): 353.     CrossRef

Mechanical properties and microleakage of two composites [conventional hybrid type DenFil (VERICOM Co., Anyang, Korea) / micro matrix hybrid type Esthet X (Dentsply Caulk, Milford, DE, U.S.A.)] were evaluated to assess whether variable light intensity curing is better than conventional curing technique.

Curing was done for 40 seconds in two ways of 2 step soft-start technique and 5 step ramping technique. Three kinds of light intensities of 50, 100, 200 mW/cm² were initially used for 10, 20, 30 seconds each and the maximum intensity of 600 mW/cm² was used for the rest of curing time in a soft-start curing technique. In a ramping technique, curing was done with the same initial intensities and the light intensity was increased 5 times with the same rate to the maximum intensity of 600 mW/cm².

After determining conditions that showed no different mechanical properties with conventional technique, Esthet X composite was filled in a class V cavity, which dimension was 4×3×1.5 mm and cured under those conditions.

Microleakage was evaluated in two ways of dye penetration and maximum gap estimation through SEM observation. ANOVA and Spearman's rho test were used to confirm any statistical significance among groups.

The results were as follows:

Several curing conditions of variable light intensities resulted in the similar mechanical properties with a conventional continuous curing technique, except conditions that start curing with an initial light intensity of 50 mW/cm²,

From the results of this study, it was revealed that ramping technique would be better than conventional technique in mechanical properties, however, soft-start technique might be better than conventional one in microleakage.

It was concluded that much endeavor should be made to find out the curing conditions, which have advantages of both aspects or to solve these kinds of problems through a novel idea of polymerization.

Several ways of curing are being tried to improve material’s properties and reduce marginal gap. However, all are considering about the pattern of light intensity. It was noted from the preliminary study the change of light wavelength from filter changing may give an impact on material’s property and microleakage.

The object of this study was to verify the effect of filters with various wavelength width on the microhardness and microleakage of composite resin; hybrid type of DenFil and submicron hybrid type of Esthet X. Composite resins were cured using 3 kinds of filter; narrow-banded(465-475 nm), mid-banded(430-470 nm), wide-banded(400-500 nm). After the estimation of microhardness, degree of dye penetration and the maximum gap from SEM evaluation were done between 4 groups that showed no difference in microhardness value of the lower surface.

The results were as follows:

Adequate microhardness could not be gained with a narrow-banded filter irrespective of curing time. At the upper surface, DenFil should be polymerized with middle or wide-banded filter for 20 seconds at least, while Esthet X be cured with middle or wide-banded filter for 30 seconds at least to get similar hardness value to control group.

From these results, it could be concluded that curing with wide-width filter would be better than the other techniques, even though the curing technique using mid-width filter seems to have its own unique advantage.

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• The Effect of Two Different Light-Curing Units and Curing Times on Bulk-Fill Restorative Materials
  Gokcen Deniz Bayrak, Elif Yaman-Dosdogru, Senem Selvi-Kuvvetli
  Polymers.2022; 14(9): 1885.     CrossRef