Microtensile bond strength of single step adhesives to dentin

Young-Gon Cho; Young-Jae Kee

doi:10.5395/JKACD.2005.30.4.312

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Original Article Microtensile bond strength of single step adhesives to dentin: Young-Gon Cho, Young-Jae Kee; Journal of Korean Academy of Conservative Dentistry 2005;30(4):312-318.
DOI: https://doi.org/10.5395/JKACD.2005.30.4.312
Published online: July 30, 2005

Department of Conservative Dentistry, College of Dentistry, Chosun University, Korea.

Corresponding author: Young-Gon Cho. Department of Conservative Dentistry, College of Dentistry, Chosun University, 421 Seosuk-dong, Dong-gu, Gwangju, Korea, 501-825. Tel: 82-62-220-3840, 3845, Fax: 82-62-232-9064, ygcho@mail.chosun.ac.kr

• Received: December 24, 2004 • Revised: February 18, 2005 • Accepted: March 5, 2005

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Abstract
REFERENCES

Abstract

This study compared the microtensile bond strength (µTBS) of three single step adhesives to dentin.

Occlusal superficial dentin was exposed in fifteen human molars. They were assigned to three groups by used adhesives: Xeno group (Xeno III), Prompt group (Adper Prompt L-Pop), AQ group (AQ Bond).

Each adhesive was applied to dentin surface, and composite of same manufacturer was constructed. The bonded specimens were sectioned into sticks with an interface area approximately 1 mm², and subjected to µTBS testing with a crosshead speed of 1 mm/minute. The results of this study were as follows;

The µTBS to dentin was 48.78 ± 9.83 MPa for Xeno III, 30.22 ± 4.52 MPa for Adper Prompt L-Pop, and 26.31 ± 7.07 MPa for AQ Bond.

The mean µTBS of Xeno group was significantly higher than that of Prompt group and AQ group (p < 0.05).

There was no significant difference between the µTBS of Prompt group and AQ group.
Keywords: Microtensile bond strength (µTBS); Single step adhesives; Superficial dentin; Interface area

REFERENCES

1. Toledano M, Perdigao J, Osorio E. Influence of NaOCL deproteinization on shear bond strength in function of dentin depth. Am J Dent. 2002;15: 252-255.PubMed
2. Cho YG, Jeong JH, Ki YJ, Choi HY, Jin CH, Yoo SH, Kim JU, Park BC. Marginal microleakage of single step adhesives. J Korean Acad Conserv Dent. 2004;29: 162-169.
3. Medina VO, Shinkai K, Shirono M, Tanaka N, Katoh Y. Histopathologic study on pulp response to single-bottle and self-etching adhesive systems. Oper Dent. 2002;27: 330-342.PubMed
4. Toba S, Veerapravati W, Shimada Y, Nikaido T, Tagami J. Microshear bond strengths of adhesive resins to coronal dentin versus the floor of the pulp chamber. Am J Dent. 2003;16: 51A-56A.PubMed
5. Cardoso PE, Braga RR, Carrilho MR. Evaluation of micro-tensile, shear and tensile tests determining the bond strength of three adhesive systems. Dent Mater. 1998;14: 394-398.Article PubMed
6. Perdigao J, Frankenberger R, Rosa BT, Breschi L. New trends in dentin/enamel adhesion. Am J Dent. 2000;13: 25D-30D.PubMed
7. Miyazaki M, Mikitake S, Onose H, Moore BK. Influence of thermal cycling on dentin bond strength of two-step bonding systems. Am J Dent. 1998;11: 118-122.PubMed
8. Akagawa H, Nikaido T, Takada T, Burrow MF, Tagami J. Shear bond strengths to coronal and pulp chamber floor dentin. Am J Dent. 2002;15: 383-388.PubMed
9. Sano H, Shono T, Sonoda H, Takatsu T, Ciucchi B, Carvalho RM. Pashley DH. Relationship between surface area for adhesion and tensile bond strength-evaluation of micro-tensile bond test. Dent Mater. 1994;10: 236-240.PubMed
10. Phrukkanon S, Burrow MF, Tyas MJ. The influence of cross-sectional shape and surface area on the microtensile bond test. Dent Mater. 1998;14: 212-221.Article PubMed
11. Pashley DH, Sano H, Ciucchi B, Yoshiyama M, Carvalho RM. Adhesion testing of dentin bonding agents: a review. Dent Mater. 1995;11: 117-125.Article PubMed
12. Toledano M, Osorio R, Ceballos L, Fuentes MV, Fernandes CAO, Tay FR, Carvalho RM. Microtensile bond strength of several adhesive systems to different dentin depths. Am J Dent. 2003;16: 292-298.PubMed
13. De Munck J, Van Meerbeek B, Satoshi I, Vargas M, Yoshida Y, Armstrong S, Lambrechts P, Vanherle G. Microtensile bond strengths of one- and two-step self-etch adhesives to bur-cut enamel and dentin. Am J Dent. 2003;16: 414-420.PubMed
14. Brunton PA, Cowan AJ, Wilson MA. A three-year evaluation of restorations placed with smear-layer-mediated dentin bonding agent in non-carious cervical lesions. J Adhes Dent. 1999;1: 333-341.PubMed
15. Inoue S, Vargas MA, Abe Y, Yoshida Y, Lambrechts P, Vanherle G, Sano H, Van Meerbeek B. Microtensile bond strength of eleven contemporary adhesives to dentin. J Adhes Dent. 2001;3: 237-245.PubMed
16. Perdigao J. Dentin bonding as a function of dentin structure. Dent Clin North Am. 2002;46: 277-301.Article PubMed
17. Ikemura K, Koura Y, Endo T. Effect of 4-acryloxyethyltrimellitic acid in a self-etching primer on bonding to ground dentine. Dent Mater J. 1996;15: 132-143.PubMed
18. Koibuchi H, Yasuda N, Nakabayashi N. Bonding to dentin with a self-etching primer: The effect of smear layer. Dent Mater. 2001;17: 122-126.PubMed
19. Tay FR, Pashley DH. Aggressiveness of contemporary self-etching adhesives. I: Depth of penetration beyond dentin smear layers. Dent Mater. 2001;17: 296-308.PubMed
20. Camps J, Pashley DH. Buffering action of human dentin in vitro. J Adhes Dent. 2000;2: 39-50.PubMed
21. Nakabayashi N, Saimi Y. Bonding to intact dentin. J Dent Res. 1996;75: 1706-1715.Article PubMed PDF
22. Tay FR, Pashley DH, Peters MC. Adhesive permeability affects composite coupling to dentin treated with a self-etch adhesive. Oper Dent. 2003;28: 610-621.PubMed
23. Chan KM, Tay FR, King NM, Imazato S, Pashley DH. Bonding of mild self-etching primers/adhesives to dentin with thick smear layers. Am J Dent. 2003;16: 340-346.PubMed
24. Watanabe I, Saimi Y, Nakabayashi N. Effect of smear layer on bonding to ground dentin-Relationship between griding condition and tensile bond strength. J Jpn Soc Dent Mater Devices. 1994;13: 101-108.
25. Cheong C, King NM, Pashley DH, Ferrari M, Toledano M, Tay FR. Incompatibility of self-etch adhesives with chemical/dual-cured composites: two-step vs one-step systems. Oper Dent. 2003;28: 747-755.PubMed
26. Miyazaki M, Iwasaki K, Onose H. Adhesion of single application bonding systems to bovine enamel and dentin. Oper Dent. 2002;27: 88-94.PubMed
27. Frankenberger R, Perdigao J, Rosa BT, Lopes M. "No-bottle" vs "multi-bottle" dentin adhesives- a microtensile bond strength and morphological study. Dent Mater. 2001;17: 373-380.Article PubMed
28. Inoue H, Inoue S, Uno S, Takahashi A, Koase K, Sano H. Micro-tensile bond strength of two single-step adhesive systems to bur-prepared dentin. J Adhes Dent. 2001;3: 129-136.PubMed

Figure 1

Specimen adhered to the testing apparatus.

Figure 2

EZ test for microtensile bond strength test.

Table 1

The components and pH of single step adhesives and composites

HEMA: 2 hydroxyethyl methacrylate, Pyro-EMA: tetramethacryloxyethyl pyrophophate, PEM-F: pentamethacryloxyethyl cyclophophazen mono fluoride, UDMA: urethane dimeth-acrylate, BHT: 2,6-Di-tert-butyl-p hydroxyl toluene, EPD: p-dimethylamino ethyl benzoate, Bis-GMA: Bisphenol glycidyl methacrylate, 4-META: 4-metha-cryloxyethyl trimellitate anhydride, PTS: p-toluensulfinic acid sodium salt

Table 2

Mean microtensile bond strength of each group (Unit: MPa, Mean ± S.D.)

Superscripts of the different letters indicate values of statistical significant difference (p < 0.05, Tukey test).

Tables & Figures

REFERENCES

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Microtensile bond strength of single step adhesives to dentin

J Korean Acad Conserv Dent. 2005;30(4):312-318. Published online July 30, 2005

DOI: https://doi.org/10.5395/JKACD.2005.30.4.312

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Figure

Microtensile bond strength of single step adhesives to dentin

Figure 1 Specimen adhered to the testing apparatus.

Figure 2 EZ test for microtensile bond strength test.

Figure 1

Figure 2

Microtensile bond strength of single step adhesives to dentin

Table 1

The components and pH of single step adhesives and composites

Table 2

Mean microtensile bond strength of each group (Unit: MPa, Mean ± S.D.)

Superscripts of the different letters indicate values of statistical significant difference (p < 0.05, Tukey test).

Table 1 The components and pH of single step adhesives and composites

Table 2 Mean microtensile bond strength of each group (Unit: MPa, Mean ± S.D.)

Superscripts of the different letters indicate values of statistical significant difference (p < 0.05, Tukey test).