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Compatibility of self-etching dentin adhesives with resin luting cements
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Original Article Compatibility of self-etching dentin adhesives with resin luting cements
Do-Wan Kim, Sang-Jin Park, Kyoung-Kyu Choi
Journal of Korean Academy of Conservative Dentistry 2005;30(6):493-504.
DOI: https://doi.org/10.5395/JKACD.2005.30.6.493
Published online: November 30, 2005

Department of Conservative Dentistry, Division of Dentistry, Graduate School, Kyung Hee University, Korea.

Corresponding Author: Kyoung-Kyu Choi. Department of Conservative Dentistry, Division of Dentistry, Graduate School, Kyung Hee University, 1, Hoegi Dong, Dongdaemun Gu, Seoul, Korea, 130-702. Tel: 82-2-958-9337, choikkyu@khu.ac.kr
• Received: August 9, 2005   • Revised: October 6, 2005   • Accepted: October 20, 2005

Copyright © 2005 Korean Academy of Conservative Dentistry

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  • This study was performed to investigate the compatibility between 4 dentin adhesives and 4 resin luting cements.
    Dentin adhesives used in this study were All-Bond 2 (Bisco Inc., Schaumbrug, IL, USA), Clearfil SE-Bond (Kuraray Medical Inc, Osaka, Japan), Prompt L-Pop (3M Dental Products, St. Paul, MN, USA), One-Up Bond F (Tokuyama corp., Tokyo, Japan). Resin luting cements used in this study were Choice (Bisco Inc., Schaumbrug, IL, USA), Panavia F (Kuraray Medical Inc, Osaka, Japan), RelyX ARC (3M Dental Products, St. Paul, MN, USA), Bistite II DC (Tokuyama corp., Tokyo, Japan). Combination of each dentin adhesive and corresponding resin cement was made to 16 experimental groups.
    Flat dentin surfaces was created on mid-coronal dentin of extracted mandibular third molars, then dentin surface was polished with 320-grit silicon carbide abrasive papers.
    Indirect resin composite block (Tescera, Bisco) was fabricated. Its surface for bonding to tooth was polished with silicon carbide abrasive papers. Each dentin adhesive was treated on tooth surface and resin composite overlay were luted with each resin cement. Each bonded specimen was poured in epoxy resin and sectioned occluso-gingivally into 1.0 mm thick slab, then further sectioned into 1.0 × 1.0 mm2 composite-dentin beams. Microtensile bond strength was tested at a crosshead speed of 1.0 mm/min. The data were analysed by one-way ANOVA and Duncan's multiple comparison tests.
    The results of this study were as follows;
    2-step self-etching dentin adhesive which has additional bonding resin is more compatible than 1-step self-etching dentin adhesive.
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Figure 1
Schematic representation of micro-tensile bond strength test.
jkacd-30-493-g001.jpg
Figure 2
Micro-tensile bond strengths with CH resin cement.
jkacd-30-493-g002.jpg
Figure 3
Micro-tensile bond strengths with PA resin cement.
jkacd-30-493-g003.jpg
Figure 4
Micro-tensile bond strengths with RE resin cement.
jkacd-30-493-g004.jpg
Figure 5
Micro-tensile bond strengths with BI resin cement.
jkacd-30-493-g005.jpg
Figure 6
Micro-tensile bond strengths of each dentin adhesive coupled with four resin cements.
jkacd-30-493-g006.jpg
Figure 7
SEM photograph of the adhesive interface of CH-AB. Hybrid layer is well formed and resin tags are infiltrated into dentinal tubules deeply.
jkacd-30-493-g007.jpg
Figure 8
SEM photograph of the adhesive interface of BI-AB. Hybrid layer is well formed and resin tags are infiltrated into dentinal tubules deeply.
jkacd-30-493-g008.jpg
Figure 9
SEM photograph of the adhesive interface of PA-SE. Hybrid layer is well formed and resin tags are infiltrated into dentinal tubules deeply.
jkacd-30-493-g009.jpg
Figure 10
SEM photograph of the adhesive interface of RE-SE. Hybrid layer is well formed and resin tags are infiltrated into dentinal tubules deeply.
jkacd-30-493-g010.jpg
Figure 11
SEM photograph of the adhesive interface of PA-PL. Hybrid layer is relatively thin, resin tags are rare and short.
jkacd-30-493-g011.jpg
Figure 12
SEM photograph of the adhesive interface of RE-PL. Hybrid layer is formed limitedly and resin tags are rare.
jkacd-30-493-g012.jpg
Figure 13
SEM photograph of the adhesive interface of CH-OU. Resin tags are poorly formed.
jkacd-30-493-g013.jpg
Figure 14
SEM photograph of the adhesive interface of BI-OU. Few resin tags are observed.
jkacd-30-493-g014.jpg
Table 1
Dentin adhesives used in this study
jkacd-30-493-i001.jpg
Table 2
Resin cements used in this study
jkacd-30-493-i002.jpg
Table 3
Experimental Groups
jkacd-30-493-i003.jpg
Table 4
Instruction for dentin adhesive systems
jkacd-30-493-i004.jpg
Table 5
Instruction for resin cements
jkacd-30-493-i005.jpg
Table 6
Micro-tensile bond strength of dentin adhesives with resin luting cements (Mean stength ± SD MPa)

Groups with the same superscripts are not statistically significant (p = 0.05).

jkacd-30-493-i006.jpg

Tables & Figures

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        Compatibility of self-etching dentin adhesives with resin luting cements
        J Korean Acad Conserv Dent. 2005;30(6):493-504.   Published online November 30, 2005
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      Compatibility of self-etching dentin adhesives with resin luting cements
      Image Image Image Image Image Image Image Image Image Image Image Image Image Image
      Figure 1 Schematic representation of micro-tensile bond strength test.
      Figure 2 Micro-tensile bond strengths with CH resin cement.
      Figure 3 Micro-tensile bond strengths with PA resin cement.
      Figure 4 Micro-tensile bond strengths with RE resin cement.
      Figure 5 Micro-tensile bond strengths with BI resin cement.
      Figure 6 Micro-tensile bond strengths of each dentin adhesive coupled with four resin cements.
      Figure 7 SEM photograph of the adhesive interface of CH-AB. Hybrid layer is well formed and resin tags are infiltrated into dentinal tubules deeply.
      Figure 8 SEM photograph of the adhesive interface of BI-AB. Hybrid layer is well formed and resin tags are infiltrated into dentinal tubules deeply.
      Figure 9 SEM photograph of the adhesive interface of PA-SE. Hybrid layer is well formed and resin tags are infiltrated into dentinal tubules deeply.
      Figure 10 SEM photograph of the adhesive interface of RE-SE. Hybrid layer is well formed and resin tags are infiltrated into dentinal tubules deeply.
      Figure 11 SEM photograph of the adhesive interface of PA-PL. Hybrid layer is relatively thin, resin tags are rare and short.
      Figure 12 SEM photograph of the adhesive interface of RE-PL. Hybrid layer is formed limitedly and resin tags are rare.
      Figure 13 SEM photograph of the adhesive interface of CH-OU. Resin tags are poorly formed.
      Figure 14 SEM photograph of the adhesive interface of BI-OU. Few resin tags are observed.
      Compatibility of self-etching dentin adhesives with resin luting cements

      Dentin adhesives used in this study

      Resin cements used in this study

      Experimental Groups

      Instruction for dentin adhesive systems

      Instruction for resin cements

      Micro-tensile bond strength of dentin adhesives with resin luting cements (Mean stength ± SD MPa)

      Groups with the same superscripts are not statistically significant (p = 0.05).

      Table 1 Dentin adhesives used in this study

      Table 2 Resin cements used in this study

      Table 3 Experimental Groups

      Table 4 Instruction for dentin adhesive systems

      Table 5 Instruction for resin cements

      Table 6 Micro-tensile bond strength of dentin adhesives with resin luting cements (Mean stength ± SD MPa)

      Groups with the same superscripts are not statistically significant (p = 0.05).


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