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Basic Research
Physical properties of novel composite using Portland cement for retro-filling material
Sang-Jin Lee, Ok-In Cho, Jiwan Yum, Jeong-Kil Park, Bock Hur, Hyeon-Cheol Kim
J Korean Acad Conserv Dent 2010;35(6):445-452.   Published online November 30, 2010
DOI: https://doi.org/10.5395/JKACD.2010.35.6.445
AbstractAbstract PDFPubReaderePub
Objectives

The aim of this study was to compare apical sealing ability and physical properties of MTA, MTA - AH-plus mixture (AMTA) and experimental Portland cement - Epoxy resin mixture (EPPC) for a development of a novel retro-filling material.

Materials and Methods

Forty-nine extracted roots were instrumented and filled with gutta-percha. Apical root was resected at 3 mm and the retro-filling cavity was prepared for 3 mm depth. Roots were randomly divided into 3 groups of 15 roots each. The retro-filling was done using MTA, AMTA, and EPPC as the groups divided. Four roots were used as control groups. After setting in humid condition for 24 hours, the roots were immersed in 1% methylene blue dye solution for 72 hours to test the apical leakage. After immersion, the roots were vertically sectioned and photos were taken to evaluate microleakage. Setting times were measured with Vicat apparatus and digital radiographs were taken to evaluate aluminum equivalent thickness using aluminum step wedge. The results of microleakage and setting time were compared between groups using one-way ANOVA and Scheffe's post-hoc comparison at the significance level of 95%.

Results

AMTA and EPPC showed less microleakage than MTA group (p < 0.05). AMTA showed the highest radio-opacity than other groups and the novel EPPC showed 5 mm aluminum thickness radio-opacity. EPPC showed the shortest initial and final setting times than other groups while the MTA showed the longest (p < 0.05).

Conclusions

Under the condition of this study, the novel composite using Portland cement-Epoxy resin mixture may useful for retro-filling with the properties of favorable leakage resistance, radio-opacity and short setting time.

Citations

Citations to this article as recorded by  
  • Comparison of Setting Time, Compressive Strength, Solubility, and pH of Four Kinds of MTA
    Jing-Ling Che, Jae-Hwan Kim, Seon-Mi Kim, Nam-ki Choi, Hyun-Joo Moon, Moon-Jin Hwang, Ho-Jun Song, Yeong-Joon Park
    Korean Journal of Dental Materials.2016; 43(1): 61.     CrossRef
  • Biological Effects and Washout Resistance of a Newly Developed Fast-setting Pozzolan Cement
    Yoorina Choi, Su-Jung Park, Seoung-Hoon Lee, Yun-Chan Hwang, Mi-Kyung Yu, Kyung-San Min
    Journal of Endodontics.2013; 39(4): 467.     CrossRef
  • 172 View
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  • 2 Crossref
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Short Communication
Mineral trioxied aggregate and its substitutes
Yong-Bum Cho
J Korean Acad Conserv Dent 2010;35(3):149-151.   Published online May 31, 2010
DOI: https://doi.org/10.5395/JKACD.2010.35.3.149
AbstractAbstract PDFPubReaderePub

Since its introduction in 1993, Mineral Trioxide Aggregate (MTA) has been shown to be superior to others in sealing, biocompatibility, and many other aspects of clinical endodontics. MTA is primarily Portland cement with bismuth oxide as a radiopacitifier.

Although some studies suggested that the reasonable-priced Portland cement could be used instead of MTA, but MTAs are different from Portland cement in its composition, especially in heavy metal contents. Therefore, clinicians should be meticulous adapting the Portland cement as a MTA substitute.

Citations

Citations to this article as recorded by  
  • Endodontic management of a maxillary lateral incisor with dens invaginatus and external root irregularity using cone-beam computed tomography
    Young-Jun Lim, Sook-Hyun Nam, Sung-Ho Jung, Dong-Ryul Shin, Su-Jung Shin, Kyung-San Min
    Restorative Dentistry & Endodontics.2012; 37(1): 50.     CrossRef
  • 168 View
  • 1 Download
  • 1 Crossref
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Original Articles
A bioactivity study of Portland cement mixed with β-glycerophosphosphate on human pulp cell
Young-Hwan Oh, Young-Joo Jang, Yong-Bum Cho
J Korean Acad Conserv Dent 2009;34(5):415-423.   Published online September 30, 2009
DOI: https://doi.org/10.5395/JKACD.2009.34.5.415
AbstractAbstract PDFPubReaderePub

The purpose of this study is to investigate the response of human pulp cell on Portland cement mixed with β-glycerophosphate. To investigate the effect of β-glycerophosphate and/or dexamethasone on human pulp cell, ALP activity on various concentration of β-glycerophosphate and dexamethasone was measured and mineral nodule of human pulp cell was stained with Alizarin red S. MTS assay and ALP activity of human pulp cell on Portland cement mixed with various concentration of β-glycerophosphate (10 mM, 100mM, 1M) was measured and the specimens were examined under SEM.

Addition of β-glycerophosphate or dexamethasone alone had no effect however, the addition of 5 mM β-glycerophosphate and 100 nM dexamethasone had the largest increasement in ALP activity. There was no toxicity in all samples and the data showed that Portland cement mixed with 10 mM β-glycerophosphate had more increase in ALP activity compared with control.

In conclusion, Portland cement mixed with β-glycerophosphate has no toxicity and promotes differentiation and mineralization of pulp cell compared with additive-free Portland cement. This implicated that application of Portland cement mixed with β-glycerophosphate might form more reparative dentin and in turn it would bring direct pulp capping to success.

Citations

Citations to this article as recorded by  
  • Dentinogenic potential of human adult dental pulp cells during the extended primary culture
    Jin-Hee Min, Seon-Yle Ko, Yong-Bum Cho, Chun-Jeih Ryu, Young-Joo Jang
    Human Cell.2011; 24(1): 43.     CrossRef
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Comparison of biocompatibility of four root perforation repair materials
Min-Kyung Kang, In-Ho Bae, Jeong-Tae Koh, Yun-Chan Hwang, In-Nam Hwang, Won-Mann Oh
J Korean Acad Conserv Dent 2009;34(3):192-198.   Published online May 31, 2009
DOI: https://doi.org/10.5395/JKACD.2009.34.3.192
AbstractAbstract PDFPubReaderePub

This study was carried out in order to determine in vitro biocompatibility of white mineral trioxide aggregate (MTA), and to compare it with that of the commonly used materials, i. e. calcium hydroxide liner (Dycal), glass ionomer cement (GIC), and Portland cement which has a similar composition of MTA. To assess the biocompatibility of each material, cytotoxicity was examined using MG-63 cells. The degree of cytotoxicity was evaluated by scanning electron microscopy (SEM) and a colorimetric method, based on reduction of the tetrazolium salt 2,3 bis {2methoxy 4nitro 5[(sulfenylamino) carbonyl] 2H tetrazolium hydroxide} (XTT) assay.

The results of SEM revealed the cells in contact with GIC, MTA, and Portland cement at 1 and 3 days were apparently healthy. In contrast, cells in the presence of Dycal appeared rounded and detached. In XTT assay, the cellular activities of the cells incubated with all the test materials except Dycal were similar, which corresponded with the SEM observation. The present study supports the view that MTA is a very biocompatible root perforation repair material. It also suggests that cellular response of Portland cement and GIC are very similar to that of MTA.

Citations

Citations to this article as recorded by  
  • The effect of several root-end filling materials on MG63 osteoblast-like cells
    Jeong-Ho Lee, Won-Jun Shon, WooCheol Lee, Seung-Ho Baek
    Journal of Korean Academy of Conservative Dentistry.2010; 35(3): 222.     CrossRef
  • Biocompatibility of experimental mixture of mineral trioxide aggregate and glass ionomer cement
    Min-Jae Oh, Yu-Na Jeong, In-Ho Bae, So-Young Yang, Bum-Jun Park, Jeong-Tae Koh, Yun-Chan Hwang, In-Nam Hwang, Won-Mann Oh
    Journal of Korean Academy of Conservative Dentistry.2010; 35(5): 359.     CrossRef
  • Physical and chemical properties of experimental mixture of mineral trioxide aggregate and glass ionomer cement
    Yu-Na Jeong, So-Young Yang, Bum-Jun Park, Yeong-Joon Park, Yun-Chan Hwang, In-Nam Hwang, Won-Mann Oh
    Journal of Korean Academy of Conservative Dentistry.2010; 35(5): 344.     CrossRef
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  • 3 Crossref
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Ingredients and cytotoxicity of MTA and 3 kinds of Portland cements
Seok-Woo Chang, Hyun-Mi Yoo, Dong Sung Park, Tae-Seok Oh, Kwang-Shik Bae
J Korean Acad Conserv Dent 2008;33(4):369-376.   Published online July 31, 2008
DOI: https://doi.org/10.5395/JKACD.2008.33.4.369
AbstractAbstract PDFPubReaderePub

The aim of this study was to compare the compositions and cytotoxicity of white ProRoot MTA (white mineral trioxide aggregate) and 3 kinds of Portland cements. The elements, simple oxides and phase compositions of white MTA (WMTA), gray Portland cement (GPC), white Portland cement (WPC) and fast setting cement (FSC) were measured by inductively coupled plasma atomic emission spectrometry (ICP-AES), X-ray fluorescence spectrometry (XRF) and X-ray diffractometry (XRD). Agar diffusion test was carried out to evaluate the cytotoxicity of WMTA and 3 kinds of Portland cements.

The results showed that WMTA and WPC contained far less magnesium (Mg), iron (Fe), manganese (Mn), and zinc (Zn) than GPC and FSC. FSC contained far more aluminum oxide (Al2O3) than WMTA, GPC, and WPC. WMTA, GPC, WPC and FSC were composed of main phases, such as tricalcicium silicate (3CaO·SiO2), dicalcium silicate (2CaO·SiO2), tricalcium aluminate (3CaO·Al2O3), and tetracalcium aluminoferrite (4CaO·Al2O3·Fe2O3). The significance of the differences in cellular response between WMTA, GPC, WPC and FSC was statistically analyzed by Kruskal-Wallis Exact test with Bonferroni's correction. The result showed no statistically significant difference (p > 0.05).

WMTA, GPC, WPC and FSC showed similar compositions. However there were notable differences in the content of minor elements, such as aluminum (Al), magnesium, iron, manganese, and zinc. These differences might influence the physical properties of cements.

Citations

Citations to this article as recorded by  
  • Development of Multi-functional Composite Cement with Strength Improvement Using Disposable Waste Masks
    Jong-Won Chung, Hyun-Kyoung Yang
    Journal of Power System Engineering.2022; 26(3): 31.     CrossRef
  • The effects of mineral trioxide aggregate on osteo/odontogenic potential of mesenchymal stem cells: a comprehensive and systematic literature review
    Danial Babaki, Sanam Yaghoubi, Maryam M. Matin
    Biomaterial Investigations in Dentistry.2020; 7(1): 175.     CrossRef
  • Remineralization of demineralized dentin using a dual analog system
    Neha Saxena, Stefan Habelitz, Grayson W. Marshall, Laurie B. Gower
    Orthodontics & Craniofacial Research.2019; 22(S1): 76.     CrossRef
  • Chemical analysis and biological properties of two different formulations of white portland cements
    Hany Mohamed Aly Ahmed, Norhayati Luddin, Thirumulu Ponnuraj Kannan, Khairani Idah Mokhtar, Azlina Ahmad
    Scanning.2016; 38(4): 303.     CrossRef
  • In vitrocytotoxicity of four calcium silicate-based endodontic cements on human monocytes, a colorimetric MTT assay
    Sedigheh Khedmat, Somayyeh Dehghan, Jamshid Hadjati, Farimah Masoumi, Mohammad Hossein Nekoofar, Paul Michael Howell Dummer
    Restorative Dentistry & Endodontics.2014; 39(3): 149.     CrossRef
  • Conservative approach of a symptomatic carious immature permanent tooth using a tricalcium silicate cement (Biodentine): a case report
    Cyril Villat, Brigitte Grosgogeat, Dominique Seux, Pierre Farge
    Restorative Dentistry & Endodontics.2013; 38(4): 258.     CrossRef
  • Chemical characteristics of mineral trioxide aggregate and its hydration reaction
    Seok-Woo Chang
    Restorative Dentistry & Endodontics.2012; 37(4): 188.     CrossRef
  • Physical and chemical properties of experimental mixture of mineral trioxide aggregate and glass ionomer cement
    Yu-Na Jeong, So-Young Yang, Bum-Jun Park, Yeong-Joon Park, Yun-Chan Hwang, In-Nam Hwang, Won-Mann Oh
    Journal of Korean Academy of Conservative Dentistry.2010; 35(5): 344.     CrossRef
  • Biocompatibility of bioaggregate cement on human pulp and periodontal ligament (PDL) derived cells
    Choo-Ryung Chung, Euiseong Kim, Su-Jung Shin
    Journal of Korean Academy of Conservative Dentistry.2010; 35(6): 473.     CrossRef
  • Physical properties of novel composite using Portland cement for retro-filling material
    Sang-Jin Lee, Ok-In Cho, Jiwan Yum, Jeong-Kil Park, Bock Hur, Hyeon-Cheol Kim
    Journal of Korean Academy of Conservative Dentistry.2010; 35(6): 445.     CrossRef
  • A bioactivity study of Portland cement mixed with β-glycerophosphosphate on human pulp cell
    Young-Hwan Oh, Young-Joo Jang, Yong-Bum Cho
    Journal of Korean Academy of Conservative Dentistry.2009; 34(5): 415.     CrossRef
  • Comparison of biocompatibility of four root perforation repair materials
    Min-Kyung Kang, In-Ho Bae, Jeong-Tae Koh, Yun-Chan Hwang, In-Nam Hwang, Won-Mann Oh
    Journal of Korean Academy of Conservative Dentistry.2009; 34(3): 192.     CrossRef
  • Effects of condensation techniques and canal sizes on the microleakage of orthograde MTA apical plug in simulated canals
    Deuk-Lim Nam, Jeong-Kil Park, Bock Hur, Hyeon-Cheol Kim
    Journal of Korean Academy of Conservative Dentistry.2009; 34(3): 208.     CrossRef
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  • 13 Crossref
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