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Original Article The effect of additional enamel etching on microleakage of the adhesion of self-etching primer system
Jung-Jin Yoon, Kyung-San Min, Chan-Ui Hong
2003;28(5):-368.
DOI: https://doi.org/10.5395/JKACD.2003.28.5.363
Published online: September 30, 2003

Department of Conservative Dentistry, College of Dentistry, Dankook University, Korea.

Corresponding author (endohong@hanmail.net)

Copyright © 2003 Korean Academy of Conservative Dentistry

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  • The purpose of this study is to evaluate the effect of additional enamel etching with phosphoric acid on the microleakage of the adhesion of self-etching primer system.
    Class V cavity(4 mm×3 mm×1.5 mm) preparations with all margins in enamel were prepared on buccal surface of 42 extracted human upper central incisor teeth. Prepared teeth were randomly divided into 3 groups.
    Group 1 : no additional pretreatment with 37% phosphoric acid (NE).
    Group 2 : additional pretreatment with 37% phosphoric acid for 10 seconds (E10s).
    Group 3 : additional pretreatment with 37% phosphoric acid for 20 seconds (E20s).
    The adhesives(Clearfil SE Bond®, Kuraray, Osaka, Japan) and composite resins(Clearfil AP-X®, Osaka, Kuraray, Japan) were applied following the manufacturer's instructions. All the specimens were finished with the polishing disc(3M dental product, St Paul, MN, USA), thermocycled for 500 cycles between 5℃ and 55℃ and resected apical 3-mm root. 0.028 stainless steel wire was inserted apically into the pulp chamber of each tooth and sealed into position with sticky wax. Surrounding tooth surface was covered with a nail varnish 2 times except areas 1 mm far from all the margins. After drying for one day, soaked the samples in the distilled water. Microleakage was assessed by electrochemical method(System 6514, Electrometer®, Keithley, USA) in the distilled water.
    In this study, the microleakage was the lowest in group 1(NE) and the highest in group 3(E20s)(NE<E10s<E20s). But no statistically significant differences were found(p=0.5).
    On the basis of findings from this experiment, it can be concluded that additional enamel etching has no influence on the microleakage of the adhesion of self-etching primer system.
Figure 1
Measuring method for microleakage.
jkacd-28-363-g001.jpg
Table 1
Experimental groups.
jkacd-28-363-i001.jpg
Table 2
Effect of additional enamel etching on microleakage.
jkacd-28-363-i002.jpg
Table 3
Statistical analysis between groups.
jkacd-28-363-i003.jpg
  • 1. Haller B. Recent developments in dentin bonding. Am J Dent. 2000;13(1):44-50.PubMed
  • 2. Nakamura K, Arisue K, Kajiwara M, et al. Evaluation of new type of commercially available adhesive systems-effect of total treatment for enamel and dentin. Jpn J Concerv Dent. 1996;39: 304-314.
  • 3. Ferrari M, Mannocci F, Vichi A, Davidson CL. Effect of two etching times on the sealing ability of Clearfil Liner Bond 2 in Class V restorations. Am J Dent. 1997;10(2):66-70.PubMed
  • 4. Hannig M, Reinhardt KJ, Bott B. Self-etching primer vs phosphoric acid : an alternative concept for composite-to-enamel bonding. Oper Dent. 1999;24: 172-181.PubMed
  • 5. Fritz UB, Diedrich P, Finger WJ. Self-etching primers-an alternative to the conventional acid etch technique. J Orofac Orthop. 2001;62(3):238-245.ArticlePubMedPDF
  • 6. Torii Y, Itou K, Hikasa R, et al. Enamel tensile bond strength and morphology of resin enamel interface created by acid etching system with or without moisture and self-etching priming system. J Oral Rehabil. 2002;29: 528-533.ArticlePubMed
  • 7. Kubo S, Yokota H, Sata Y, Hayashi Y. Microleakage of self-etching primers after thermal and flexural loading cycling. Am J Dent. 2001;14(3):163-169.PubMed
  • 8. Barkmeier WW, Los SA, Triolo PT Jr. Bond strengths and SEM evaluation of Clearfil Liner Bond 2. Am J Dent. 1995;8(6):289-293.PubMed
  • 9. Yoshiyama M, Matsuo T, Ebisu S, Pashley DH. Regional Bond strengths of self-etching/self-priming adhesive systems. J Dent. 1998;26: 609-616.ArticlePubMed
  • 10. Lopes GC, Baratieri LN, de Andrada MA, Vieira LC. Dental Adhesion : Present state of the art and future perspectives. Quintessence Int. 2002;33(3):213-224.PubMed
  • 11. Miyazaki M, Sato M, Onose H. Durability of enamel bond strength of simplified bonding systems. Oper Dent. 2000;25: 75-80.ArticlePubMed
  • 12. Sano H, Yoshikawa T, Pereira PN, et al. Long-term durability of dentin bonds made with a self-etching primer, in vivo. J Dent Res. 1999;78(4):906-911.ArticlePubMedPDF
  • 13. Miyazaki M, Onose H, Moore BK. Effect of operator variability on dentin bond strength of two-step bonding systems. Am J Dent. 2000;13(2):101-104.PubMed
  • 14. Ibarra G, Vargas MA, Armstrong SR, Cobbb DS. Microtensile bond strength of self-etching adhesives to ground and unground enamel. J Adhes Dent. 2002;4(2):115-124.PubMed
  • 15. Yoshiyama M, Sano H, Ebisu S, et al. Regional strengths of bonding agents to cervical sclerotic root dentin. J Dent Res. 1996;75(6):1404-1413.PubMed
  • 16. Gordan VV, Vargas MA, Denthy GE. Interfacial ultrastructure of the resin enamel region of three adhesive systems. Am J Dent. 1998;11(1):13-16.PubMed
  • 17. Ogata M, Harada N, Yamaguchi S, et al. Effects of different burs on dentin bond strengths of self-etching primer bonding systems. Oper Dent. 2001;26: 375-382.PubMed
  • 18. Sano H, Shono T, Takatsu T, Hosoda H. Microporous dentin zone beneath resin impregnated layer. Oper Dent. 1994;19: 59-64.PubMed
  • 19. Cho YG, Cho KC. Marginal microleakage of self-etching primer adhesives and a self-etching adhesive. J Korean Acad Conserv Dent. 2002;27(5):493-501.
  • 20. Osins BA, Carter JM, Shih-Levine M. Microleakage of four root canal sealer cements as determined by an electrochemical technique. Oral Surg. 1983;56(1):80-88.ArticlePubMed
  • 21. Jacobsen PH, von Fraunhofer JA. Assessment of microleakage using conductimetric technique. J Dent Res. 1975;54(1):41-48.ArticlePubMedPDF
  • 22. Jacquot BM, Panighi MM, Steinmetz P, G'sell C. Evaluation of temporary restorations' microleakage by means of electrochemical impedance measurements. J Endod. 1996;22(11):586-589.ArticlePubMed

Tables & Figures

Figure 1
Measuring method for microleakage.
jkacd-28-363-g001.jpg
Table 1
Experimental groups.
jkacd-28-363-i001.jpg
Table 2
Effect of additional enamel etching on microleakage.
jkacd-28-363-i002.jpg
Table 3
Statistical analysis between groups.
jkacd-28-363-i003.jpg

REFERENCES

  • 1. Haller B. Recent developments in dentin bonding. Am J Dent. 2000;13(1):44-50.PubMed
  • 2. Nakamura K, Arisue K, Kajiwara M, et al. Evaluation of new type of commercially available adhesive systems-effect of total treatment for enamel and dentin. Jpn J Concerv Dent. 1996;39: 304-314.
  • 3. Ferrari M, Mannocci F, Vichi A, Davidson CL. Effect of two etching times on the sealing ability of Clearfil Liner Bond 2 in Class V restorations. Am J Dent. 1997;10(2):66-70.PubMed
  • 4. Hannig M, Reinhardt KJ, Bott B. Self-etching primer vs phosphoric acid : an alternative concept for composite-to-enamel bonding. Oper Dent. 1999;24: 172-181.PubMed
  • 5. Fritz UB, Diedrich P, Finger WJ. Self-etching primers-an alternative to the conventional acid etch technique. J Orofac Orthop. 2001;62(3):238-245.ArticlePubMedPDF
  • 6. Torii Y, Itou K, Hikasa R, et al. Enamel tensile bond strength and morphology of resin enamel interface created by acid etching system with or without moisture and self-etching priming system. J Oral Rehabil. 2002;29: 528-533.ArticlePubMed
  • 7. Kubo S, Yokota H, Sata Y, Hayashi Y. Microleakage of self-etching primers after thermal and flexural loading cycling. Am J Dent. 2001;14(3):163-169.PubMed
  • 8. Barkmeier WW, Los SA, Triolo PT Jr. Bond strengths and SEM evaluation of Clearfil Liner Bond 2. Am J Dent. 1995;8(6):289-293.PubMed
  • 9. Yoshiyama M, Matsuo T, Ebisu S, Pashley DH. Regional Bond strengths of self-etching/self-priming adhesive systems. J Dent. 1998;26: 609-616.ArticlePubMed
  • 10. Lopes GC, Baratieri LN, de Andrada MA, Vieira LC. Dental Adhesion : Present state of the art and future perspectives. Quintessence Int. 2002;33(3):213-224.PubMed
  • 11. Miyazaki M, Sato M, Onose H. Durability of enamel bond strength of simplified bonding systems. Oper Dent. 2000;25: 75-80.ArticlePubMed
  • 12. Sano H, Yoshikawa T, Pereira PN, et al. Long-term durability of dentin bonds made with a self-etching primer, in vivo. J Dent Res. 1999;78(4):906-911.ArticlePubMedPDF
  • 13. Miyazaki M, Onose H, Moore BK. Effect of operator variability on dentin bond strength of two-step bonding systems. Am J Dent. 2000;13(2):101-104.PubMed
  • 14. Ibarra G, Vargas MA, Armstrong SR, Cobbb DS. Microtensile bond strength of self-etching adhesives to ground and unground enamel. J Adhes Dent. 2002;4(2):115-124.PubMed
  • 15. Yoshiyama M, Sano H, Ebisu S, et al. Regional strengths of bonding agents to cervical sclerotic root dentin. J Dent Res. 1996;75(6):1404-1413.PubMed
  • 16. Gordan VV, Vargas MA, Denthy GE. Interfacial ultrastructure of the resin enamel region of three adhesive systems. Am J Dent. 1998;11(1):13-16.PubMed
  • 17. Ogata M, Harada N, Yamaguchi S, et al. Effects of different burs on dentin bond strengths of self-etching primer bonding systems. Oper Dent. 2001;26: 375-382.PubMed
  • 18. Sano H, Shono T, Takatsu T, Hosoda H. Microporous dentin zone beneath resin impregnated layer. Oper Dent. 1994;19: 59-64.PubMed
  • 19. Cho YG, Cho KC. Marginal microleakage of self-etching primer adhesives and a self-etching adhesive. J Korean Acad Conserv Dent. 2002;27(5):493-501.
  • 20. Osins BA, Carter JM, Shih-Levine M. Microleakage of four root canal sealer cements as determined by an electrochemical technique. Oral Surg. 1983;56(1):80-88.ArticlePubMed
  • 21. Jacobsen PH, von Fraunhofer JA. Assessment of microleakage using conductimetric technique. J Dent Res. 1975;54(1):41-48.ArticlePubMedPDF
  • 22. Jacquot BM, Panighi MM, Steinmetz P, G'sell C. Evaluation of temporary restorations' microleakage by means of electrochemical impedance measurements. J Endod. 1996;22(11):586-589.ArticlePubMed

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      The effect of additional enamel etching on microleakage of the adhesion of self-etching primer system
      J Korean Acad Conserv Dent. 2003;28(5):363-368.   Published online September 30, 2003
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    The effect of additional enamel etching on microleakage of the adhesion of self-etching primer system
    Image
    Figure 1 Measuring method for microleakage.
    The effect of additional enamel etching on microleakage of the adhesion of self-etching primer system

    Experimental groups.

    Effect of additional enamel etching on microleakage.

    Statistical analysis between groups.

    Table 1 Experimental groups.

    Table 2 Effect of additional enamel etching on microleakage.

    Table 3 Statistical analysis between groups.


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