EFFECT OF DENTIN SURFACE WETNESS ON TENSILE BOND STRENGTH OF SELF ADHESIVE RESIN CEMENTS

Sung-Young Yoon; Se-Hee Park; Jin-Woo Kim; Kyung-Mo Cho

doi:10.5395/JKACD.2009.34.2.113

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Original Article EFFECT OF DENTIN SURFACE WETNESS ON TENSILE BOND STRENGTH OF SELF ADHESIVE RESIN CEMENTS: Sung-Young Yoon, Se-Hee Park, Jin-Woo Kim, Kyung-Mo Cho^,*; Journal of Korean Academy of Conservative Dentistry 2009;34(2):113-119.
DOI: https://doi.org/10.5395/JKACD.2009.34.2.113
Published online: January 14, 2009

Department of Conservative Dentistry, College of Dentistry, Kangnung National University

*Corresponding Author: Kyung-Mo Cho, Department of Conservative Dentistry College of Dentistry, Kangnung National University, 123 Chibyon-dong Gangwon-do, Korea, Tel: 82-33-640-2470 Fax: 82-33-642-6410 E-mail: drbozon@kangnung.ac.kr

• Received: December 31, 2008 • Revised: February 9, 2009 • Accepted: February 17, 2009

This is an Open Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/by-nc/3.0) which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.

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Abstract
REFERENCES
참고문헌

Abstract

The purpose of this study was to compare the tensile bond strength of several self-adhesive resin cements bonded to dentin surfaces with different wet conditions.

Three self-adhesive resin cements; Rely-X Unicem (3M ESPE, St. Paul, MN, USA), Embrace Wetbond (Pulpdent, Oakland, MA, USA), Maxcem (Kerr, Orange, CA, USA) were used. Extracted sixty human molars were used. Each self-adhesive resin cement was adhered to the dentin specimens (two rectangular sticks from each molar) in different wet conditions.

Tensile bond strength were measured using universal testing machine (EZ Test, Shimadzu corporation, Kyoto, Japan) at a crosshead speed of 1.0mm/min. After the testing, bonding failures of specimens were observed by Operative microscope (OPMI pro, Carl Zeiss, Oberkochen, Germany). T-test was used to evaluate the effect of dentin surface wetness. One-way ANOVA test was used to evaluate the tensile bond strength of self-adhesive resin cements in the same condition. Scheffe's test was used for statistical analyzing at the 95% level of confidence.

The result showed that wetness of dentin surface didn't affect tensile bond strength of self-adhesive resin cements and Maxcem showed the lowest tensile bond strength.
Keywords: Self-adhesive resin cements; Tensile bond strength; Dentin surface wetness

Figure 1.

Specimen preparation for tensile bond strength.

Figure 2.

Schematic drawing of moulds.

Table 1.

Composition of materials used in this study

Group	Composition
Rely-X Unicem	Powder: glass powder, silica, calcium hydroxide, pigment,
	substituted pyrimidine, peroxy compound, initiator.
	Liquid: methacrylated phosphoric ester, dimethacrylate,
	acetate, stabilizer, initiator
Embrace Wetbond	urethane methacrylate monomer, mono-2-methacryloyloxy ethyl, glass filler,
Embrace Wetbond	BA-30, sodium fluoride
Maxcem	GPDM, co-monomers(mono-, di-, tri-functional methacrylate monomers),
	proprietary self-curing redox activator, stabilizer, camphorquinone, barium glass fillers,
	fluoroaluminosilicate glass fillers, fumed silica

GDPM; Glycerol dimethacrylate dihydrogen phosphate

Table 2.

Handling methods of the resin cement

Group	Procedure
Rely-X Unicem	Activate the capsule for 2s and mix it for 10s (Rotomix, 3M ESPE)
Embrace Wetbond	Mix and the base and catalyst though the automix dual-barrel syringe
Maxcem	Mix the base and catalyst through the automix dual-barrel syringe

Table 3.

Means of self-adhesive resin cements according to dentin wetness

Resin cements	Dentin surface	n	Mean(MPa) ± SD
Unicem	Dry	20	2.51 ± 0.01
Unicem	Wet	20	2.51 ± 0.01
Embrace	Dry	20	2.46 ± 0.24
Embrace	Wet	20	2.51 ± 0.01
Maxcem	Dry	20	2.05 ± 0.58
Maxcem	Wet	20	2.13 ± 0.48

Table 4.

Comparison between self-adhesive resin cements on dry group

Table 5.

Comparison between self-adhesive resin cements on wet group

REFERENCES

참고문헌

1. Rueggeberg FA. From vulcanite to vinyl, a history of resins in restorative dentistry. J Prosthet Dent 87:364-379. 2002.Article PubMed
2. Peumans M, Van Meerbeek B, Lambrechts P, Vanherle G. Porcelain veneers: a reviews of the literature. J Dent 28:163-177. 2000.PubMed
3. Wood M, Kern M, Thompson VP, Romberg E. Ten-year clinical and microscopic evaluation of resin-bonded restorations. Quintessence Int 27:803-807. 1996.PubMed
4. Zhen Chun Li, Shane N. Mechanical properties of dental luting cements. J Prosthet Dent 81:597-609. 1999.Article PubMed
5. Theodore M, Harald O, Edward J. Sturdevant's art & science of operative dentistry. 5th ed.. St. Louis, USA: Mosby; p. 225-227. 2006.
6. Burke FJ, Watts DC. Fracture resistance of teeth restored with dentin-bonded crowns. Quintessence Int 23:335-340. 1994.
7. Technical data sheet: Rely X Unicem, 3M ESPE. St. Paul; USA: 2007.
8. Cecilia Goracci, Alvaro H Cury, Amerigo Cantoro, Federica Papacchini, Franklin R Tay, Marco Ferrari. Microtensile bond strength and interfacial properties of self-etching and self-adhesive resin cements used to lute composite onlay under different seating forces. J Adhes Dent 8:327-335. 2006.PubMed
9. Satoshi Oooka, Masashi Miyazaki, Akitomo Rikuta, Moor BK. Influence or polymerization mode of dual-polymerized resin direct core foundation systems on bond strengths to bovine dentin. J Prosthet Dent 92:239-244. 2004.PubMed
10. Francesca Monticelli, Marco Ferrari, Manuel Toledano. Cement system and surface treatment selection for fiber post luting. Med Oral Patol Oral Cir Bucal 13:E214-E221. 2008.PubMed
11. Technical overview: Embrace Universal resin cement. Pulpdent; Oakland USA: available at:. http://www.pulpdent.com/embraceproducts/embrace1.html. accessed Sep 23. 2008.
12. Technical bulletin: Maxcem, Kerr, Orange. USA: 2007.
13. Van Land, uyt K. L, Mine A, DeMunck J, Countinho E, Peumans M, Jaecques S, Lambrechts P, Van Meerbeek B. Techjnique sensitivity of water-free one-step adhesives. Dent Mater 24:1258-1267. 2008.PubMed
14. Jacobsen Thomas, Werner J Finger, Masafumi Kanehira. Air-건조ing time of self-etching adhesives vs bonding efficacy. J Adhes Dent 8:387-392. 2006.PubMed
15. Theodore M, Harald O, Edward J. Sturdevant's art & science of operative dentistry. 5th ed.. St. Louis, USA: Mosby; 603: p. 847-848. 2006.
16. Saygili G, Sahmali S. Effect of ceramic surface treatment on the shear bond strengths of two resin luting agents to all-ceramic materials. J Oral Rehabil 30:758-764. 2003.Article PubMed PDF
17. Abo-Hamar SE, Hiller KA, Jung H, Federlin M, Friedl KH, Schmalz G. Bond strength of a new universal self-adhesive resin luting cement to dentin and enamel. Clin Oral Invest 9:161-167. 2005.
18. 송 혜미, 박 수정, 조 현구, 황 윤찬, 오 원만, 황 인남. 치과용 접착 제가 복합레진 인레이와 레진시멘트의 결합력에 미치는 영향. 대한치과보존학회지 33:419-427. 2008.
19. 강 순일, 박 정길, 허 복, 김 현철. 부가적 부식 과정이 단일 접착 과정 레진 시멘트의 접착 강도에 미치는 영향. 대한치과보존학 회지 33:443-451. 2008.
20. DeMunk J, Vargas M, Van Landuyt K, Hikita K, Lambrechts P, Van Meerbeek B. Bonding of an auto-adhesive luting material to enamel and dentin. Dent Mater 20:963-971. 2004.Article PubMed
21. Escribano N, de la Macorra JC. Mcritensile bond strength of self-adhcesive luting cements to ceramic. J Adhes Dent 5:337-341. 2006.
22. 이 현아, 조 영곤. 다양한 레진시멘트로 합착한 섬유포스트의 결 합강도 비교. 대한치과보존학회지 33:499-506. 2008.
23. Yang B, Ludwig K, Adelung R, Kern M. Micro-tensile bond strength of three luting resins to human regional dentin. Dent Mater 22:45-56. 2006.Article PubMed
24. Radovic Ivana, Monticelli Francesca, Goracci Cecilia, Zoran R Vulicevic, Marco Ferrari. Self-adhesive resin cements: A literature review. J Adhes Dent 10:251-258. 2008.PubMed
25. Van Meerbeek B, De Munck J, Yoshida Y, Inoue S, Vargas M, Vijay P, Van Landuyt K, Lambrechts P, Vanherle G. Buonocore Memorial Lecture Adhesion to enamel and dentin: Current status and future challenges. Oper Dent 28:215-35. 2003.PubMed
26. De Munck J, Van Landuyt K, Peumans M, Poitevin A, Lambrechts P, Braem M, Van Meerbeek B. A critical review of the durability of adhesion to tooth tissue: methods and results. J Dent Res 84:118-32. 2005.Article PubMed PDF
27. Zhang ZX, Huang C, Zheng TL, Wang S, Cheng XR. Effects of residual water on microtensile bond strength of one-bottle dentin adhesive systems with different solvent bases. Chin Med J (Engl) 118:1623-1628. 2005.PubMed
28. Chiba Y, Rikuta A, Yasuda G, Yamamoto A, Takamizawa T, Kurokawa H, Ando S, Miyazaki M. Influence of moisture conditions on dentin bond strength of single-step self-etch adhesive systems. J Oral Sci 48:131-137. 2006.Article PubMed
29. Magne P, Mahallati R, Bazos P, So W.S. Direct dentin bonding technique sensitivity when using air/suction 건 조ing steps. J Esthet Restor Dent 20:130-140. 2008.PubMed
30. Gerth HU, Dammaschke T, Zuchner H, Schafer E. Chmical analysis and bonding reaction of Rely X Unicem and Bifix composites-a comparative study. Dent Mater 22:934-941. 2006.PubMed
31. Hiraishi N, Yiu CK, King NM, Tay FR. Effect of pulpal pressure on the microtensile bond strength of luting resin cements to human dentin. Dent Mater Jun 21 Epub 2008.Article PubMed
32. Hikita K, Van Meerbeek B, DeMunck J, Ikeda T, Van Landuyt K, Maida T, Lambrechts P, Peumans M. Bond effectiveness of adhesive luting agents to enamel and dentin. Dent Mater 23:71-80. 2007.PubMed
33. Favianelli A, Goracci C, Bertelli E, Monticelli F, Grandini S, Ferrari M. In vitro evaluation of wall-to-wall adaptation of a self-adhesive resin cement used for luting gold and ceramic inlays. J Adhes Dent 7:33-40. 2005.PubMed

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EFFECT OF DENTIN SURFACE WETNESS ON TENSILE BOND STRENGTH OF SELF ADHESIVE RESIN CEMENTS

J Korean Acad Conserv Dent. 2009;34(2):113-119. Published online January 14, 2009

DOI: https://doi.org/10.5395/JKACD.2009.34.2.113

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Figure

EFFECT OF DENTIN SURFACE WETNESS ON TENSILE BOND STRENGTH OF SELF ADHESIVE RESIN CEMENTS

Figure 1. Specimen preparation for tensile bond strength.

Figure 2. Schematic drawing of moulds.

Figure 1.

Figure 2.

EFFECT OF DENTIN SURFACE WETNESS ON TENSILE BOND STRENGTH OF SELF ADHESIVE RESIN CEMENTS

Group	Composition
Rely-X Unicem	Powder: glass powder, silica, calcium hydroxide, pigment,
	substituted pyrimidine, peroxy compound, initiator.
	Liquid: methacrylated phosphoric ester, dimethacrylate,
	acetate, stabilizer, initiator
Embrace Wetbond	urethane methacrylate monomer, mono-2-methacryloyloxy ethyl, glass filler,
Embrace Wetbond	BA-30, sodium fluoride
Maxcem	GPDM, co-monomers(mono-, di-, tri-functional methacrylate monomers),
	proprietary self-curing redox activator, stabilizer, camphorquinone, barium glass fillers,
	fluoroaluminosilicate glass fillers, fumed silica

Group	Procedure
Rely-X Unicem	Activate the capsule for 2s and mix it for 10s (Rotomix, 3M ESPE)
Embrace Wetbond	Mix and the base and catalyst though the automix dual-barrel syringe
Maxcem	Mix the base and catalyst through the automix dual-barrel syringe

Resin cements	Dentin surface	n	Mean(MPa) ± SD
Unicem	Dry	20	2.51 ± 0.01
Unicem	Wet	20	2.51 ± 0.01
Embrace	Dry	20	2.46 ± 0.24
Embrace	Wet	20	2.51 ± 0.01
Maxcem	Dry	20	2.05 ± 0.58
Maxcem	Wet	20	2.13 ± 0.48

Table 1. Composition of materials used in this study

GDPM; Glycerol dimethacrylate dihydrogen phosphate

Table 2. Handling methods of the resin cement

Table 3. Means of self-adhesive resin cements according to dentin wetness

Table 4. Comparison between self-adhesive resin cements on dry group

Table 5. Comparison between self-adhesive resin cements on wet group