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Research Article
Bonding of the silane containing multi-mode universal adhesive for lithium disilicate ceramics
Hyun-Young Lee, Geum-Jun Han, Juhea Chang, Ho-Hyun Son
Restor Dent Endod 2017;42(2):95-104.   Published online January 25, 2017
DOI: https://doi.org/10.5395/rde.2017.42.2.95
AbstractAbstract PDFPubReaderePub
Objectives

This study evaluated the influence of a multi-mode universal adhesive (MUA) containing silane (Single Bond Universal, 3M EPSE) on the bonding of resin cement to lithium disilicate.

Materials and Methods

Thirty IPS e.max CAD specimens (Ivoclar Vivadent) were fabricated. The surfaces were treated as follows: Group A, adhesive that did not contain silane (ANS, Porcelain Bonding Resin, Bisco); Group B, silane (S) and ANS; Group C, hydrofluoric acid (HF), S, and ANS; Group D, MUA; Group E, HF and MUA. Dual-cure resin cement (NX3, Kerr) was applied and composite resin cylinders of 0.8 mm in diameter were placed on it before light polymerization. Bonded specimens were stored in water for 24 hours or underwent a 10,000 thermocycling process prior to microshear bond strength testing. The data were analyzed using multivariate analysis of variance (p < 0.05).

Results

Bond strength varied significantly among the groups (p < 0.05), except for Groups A and D. Group C showed the highest initial bond strength (27.1 ± 6.9 MPa), followed by Group E, Group B, Group D, and Group A. Thermocycling significantly reduced bond strength in Groups B, C, and E (p < 0.05). Bond strength in Group C was the highest regardless of the storage conditions (p < 0.05).

Conclusions

Surface treatment of lithium disilicate using HF and silane increased the bond strength of resin cement. However, after thermocycling, the silane in MUA did not help achieve durable bond strength between lithium disilicate and resin cement, even when HF was applied.

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Basic Research
Effect of surface treatment of FRC-Post on bonding strength to resin cements
Chan-Hyun Park, Se-Hee Park, Jin-Woo Kim, Kyung-Mo Cho
J Korean Acad Conserv Dent 2011;36(2):125-131.   Published online March 31, 2011
DOI: https://doi.org/10.5395/JKACD.2011.36.2.125
AbstractAbstract PDFPubReaderePub
Objectives

The purpose of this study was to evaluate the effect of surface treatment of FRC-Post on bonding strength to resin cements.

Materials and Methods

Pre-surface treated LuxaPost (DMG), Rely-X Fiber Post (3M ESPE) and self adhesive resin cement Rely-X Unicem (3M ESPE), conventional resin cement Rely-X ARC (3M ESPE), and Rely-X Ceramic Primer (3M ESPE) were used. After completing the surface treatments of the posts, posts and resin cement were placed in clear molds and photo-activation was performed. The specimens were sectioned perpendicular to the FRC-Post into 2 mm-thick segments, and push-out strength were measured. The results of bond strength value were statistically analyzed using independent samples t-test and one-way ANOVA with multiple comparisons using Scheffe's test.

Results

Silanization of posts affect to the bond strength in LuxaPost, and did not affect in Rely-X Fiber Post. Rely-X ARC showed higher value than Rely-X Unicem.

Conclusions

Silanization is needed to enhance the bond strength between LuxaPost and resin cements.

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