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Mineral content analysis of root canal dentin using laser-induced breakdown spectroscopy
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Selen Küçükkaya Eren, Emel Uzunoğlu, Banu Sezer, Zeliha Yılmaz, İsmail Hakkı Boyacı
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Restor Dent Endod 2018;43(1):e11. Published online February 4, 2018
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DOI: https://doi.org/10.5395/rde.2018.43.e11
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Abstract
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- Objectives
This study aimed to introduce the use of laser-induced breakdown spectroscopy (LIBS) for evaluation of the mineral content of root canal dentin, and to assess whether a correlation exists between LIBS and scanning electron microscopy/energy dispersive spectroscopy (SEM/EDS) methods by comparing the effects of irrigation solutions on the mineral content change of root canal dentin. Materials and MethodsForty teeth with a single root canal were decoronated and longitudinally sectioned to expose the canals. The root halves were divided into 4 groups (n = 10) according to the solution applied: group NaOCl, 5.25% sodium hypochlorite (NaOCl) for 1 hour; group EDTA, 17% ethylenediaminetetraacetic acid (EDTA) for 2 minutes; group NaOCl+EDTA, 5.25% NaOCl for 1 hour and 17% EDTA for 2 minutes; a control group. Each root half belonging to the same root was evaluated for mineral content with either LIBS or SEM/EDS methods. The data were analyzed statistically. ResultsIn groups NaOCl and NaOCl+EDTA, the calcium (Ca)/phosphorus (P) ratio decreased while the sodium (Na) level increased compared with the other groups (p < 0.05). The magnesium (Mg) level changes were not significant among the groups. A significant positive correlation was found between the results of LIBS and SEM/EDS analyses (r = 0.84, p < 0.001). ConclusionsTreatment with NaOCl for 1 hour altered the mineral content of dentin, while EDTA application for 2 minutes had no effect on the elemental composition. The LIBS method proved to be reliable while providing data for the elemental composition of root canal dentin.
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- In vitro evaluation of antimicrobial photodynamic therapy with photosensitizers and calcium hydroxide on bond strength, chemical composition, and sealing of glass-fiber posts to root dentin
Thalya Fernanda Horsth Maltarollo, Paulo Henrique dos Santos, Henrique Augusto Banci, Mariana de Oliveira Bachega, Beatriz Melare de Oliveira, Marco Hungaro Antonio Duarte, Índia Olinta de Azevedo Queiroz, Rodrigo Rodrigues Amaral, Luciano Angelo Tavares Lasers in Medical Science.2025;[Epub] CrossRef - Effect of Using 5% Apple Vinegar Irrigation Solution Adjunct to Diode Laser on Smear Layer Removal and Calcium/Phosphorus Ion Ratio during Root Canal Treatment
Tarek AA Salam, Haythem SA Kader, Elsayed E Abdallah CODS - Journal of Dentistry.2024; 15(1): 3. CrossRef - Evaluation of chemical composition of root canal dentin between two age groups using different irrigating solutions: An in vitro sem-eds study
Naresh Kumar K, Abhijith Kallu, Surender L.R, Sravani Nirmala, Narender Reddy International Dental Journal of Student's Research.2024; 12(1): 18. CrossRef - Minimally invasive management of vital teeth requiring root canal therapy
E. Karatas, M. Hadis, W. M. Palin, M. R. Milward, S. A. Kuehne, J. Camilleri Scientific Reports.2023;[Epub] CrossRef - The Effects of a Novel Nanohydroxyapatite Gel and Er: YAG Laser Treatment on Dentin Hypersensitivity
Demet Sahin, Ceren Deger, Burcu Oglakci, Metehan Demirkol, Bedri Onur Kucukyildirim, Mehtikar Gursel, Evrim Eliguzeloglu Dalkilic Materials.2023; 16(19): 6522. CrossRef - Chitosan Homogenizing Coffee Ring Effect for Soil Available Potassium Determination Using Laser-Induced Breakdown Spectroscopy
Xiaolong Li, Rongqin Chen, Zhengkai You, Tiantian Pan, Rui Yang, Jing Huang, Hui Fang, Wenwen Kong, Jiyu Peng, Fei Liu Chemosensors.2022; 10(9): 374. CrossRef - Quantitative analysis of cadmium in rice roots based on LIBS and chemometrics methods
Wei Wang, Wenwen Kong, Tingting Shen, Zun Man, Wenjing Zhu, Yong He, Fei Liu Environmental Sciences Europe.2021;[Epub] CrossRef
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Effects of dentin moisture on the push-out bond strength of a fiber post luted with different self-adhesive resin cements
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Sevinç Aktemur Türker, Emel Uzunoğlu, Zeliha Yılmaz
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Restor Dent Endod 2013;38(4):234-240. Published online November 12, 2013
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DOI: https://doi.org/10.5395/rde.2013.38.4.234
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Abstract
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- Objectives
This study evaluated the effects of intraradicular moisture on the pushout bond strength of a fibre post luted with several self-adhesive resin cements. Materials and MethodsEndodontically treated root canals were treated with one of three luting cements: (1) RelyX U100, (2) Clearfil SA, and (3) G-Cem. Roots were then divided into four subgroups according to the moisture condition tested: (I) dry: excess water removed with paper points followed by dehydration with 95% ethanol, (II) normal moisture: canals blot-dried with paper points until appearing dry, (III) moist: canals dried by low vacuum using a Luer adapter, and (IV) wet: canals remained totally flooded. Two 1-mm-thick slices were obtained from each root sample and bond strength was measured using a push-out test setup. The data were analysed using a two-way analysis of variance and the Bonferroni post hoc test with p = 0.05. ResultsStatistical analysis demonstrated that moisture levels had a significant effect on the bond strength of luting cements (p < 0.05), with the exception of G-Cem. RelyX U100 displayed the highest bond strength under moist conditions (III). Clearfil SA had the highest bond strength under normal moisture conditions (II). Statistical ranking of bond strength values was as follows: RelyX U100 > Clearfil SA > G-Cem. ConclusionsThe degree of residual moisture significantly affected the adhesion of luting cements to radicular dentine.
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Citations
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Shimaa Rifaat, Ahmed Rahoma, Hind Muneer Alharbi, Sawsan Jamal Kazim, Shrouq Ali Aljuaid, Basmah Omar Alakloby, Faraz A. Farooqi, Noha Taymour Prosthesis.2025; 7(1): 18. CrossRef - Dentin bond strength of resin luting agents under a simulated intra-oral environment
Takashi Washino, Hanemi Tsuruta, Masaomi Ikeda, Michael F. Burrow, Toru Nikaido Asian Pacific Journal of Dentistry.2024; 24(2): 13. CrossRef - Effects of a relined fiberglass post with conventional and self-adhesive resin cement
Wilton Lima dos Santos Junior, Marina Rodrigues Santi, Rodrigo Barros Esteves Lins, Luís Roberto Marcondes Martins Restorative Dentistry & Endodontics.2024;[Epub] CrossRef - Effect of dentin moisture on the adhesive properties of luting fiber posts using adhesive strategies
Renata Terumi JITUMORI, Rafaela Caroline RODRIGUES, Alessandra REIS, João Carlos GOMES, Giovana Mongruel GOMES Brazilian Oral Research.2023;[Epub] CrossRef - Influence of different intraradicular chemical pretreatments on the bond strength of adhesive interface between dentine and fiber post cements: A systematic review and network meta‐analysis
Ana Luiza Barbosa Jurema, Ayla Macyelle de Oliveira Correia, Manuela da Silva Spinola, Eduardo Bresciani, Taciana Marco Ferraz Caneppele European Journal of Oral Sciences.2022;[Epub] CrossRef - SELF ADEZİV REZİN SİMANLAR / SELF ADHESIVE RESIN CEMENTS
Kübra AMAÇ, Engin ESENTÜRK, Bilge TURHAN BAL Atatürk Üniversitesi Diş Hekimliği Fakültesi Dergisi.2022; : 1. CrossRef - Postspace pretreatment with 17% ethylenediamine tetraacetic acid, 7% maleic acid, and 1% phytic acid on bond strength of fiber posts luted with a self-adhesive resin cement
PriyaC Yadav, Ramya Raghu, Ashish Shetty, Subhashini Rajasekhara Journal of Conservative Dentistry.2021; 24(6): 558. CrossRef - Development and characterization of biological bovine dentin posts
Alice Gonçalves Penelas, Eduardo Moreira da Silva, Laiza Tatiana Poskus, Amanda Cypriano Alves, Isis Ingrid Nogueira Simões, Viviane Hass, José Guilherme Antunes Guimarães Journal of the Mechanical Behavior of Biomedical Materials.2019; 92: 197. CrossRef - Evaluation of the influence of time and concentration of sodium hypochlorite on the bond strength of glass fibre post
Beau Knight, Robert M. Love, Roy George Australian Endodontic Journal.2018; 44(3): 267. CrossRef - Test methods for bond strength of glass fiber posts to dentin: A review
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Thaynara Faelly BOING, Giovana Mongruel GOMES, João Carlos GOMES, Alessandra REIS, Osnara Maria Mongruel GOMES Journal of Applied Oral Science.2017; 25(1): 2. CrossRef - A Twofold Comparison between Dual Cure Resin Modified Cement and Glass Ionomer Cement for Orthodontic Band Cementation
Hanaa El Attar, Omnia Elhiny, Ghada Salem, Ahmed Abdelrahman, Mazen Attia Open Access Macedonian Journal of Medical Sciences.2016; 4(4): 695. CrossRef - Shear bond strengths of various self-adhesive resin cements between bovine dentin and 4 types of adherends
Ah-Jin Kim, Da-Ryeong Park, Seunghan Oh, Ji-Myung Bae Korean Journal of Dental Materials.2015; 42(4): 365. CrossRef
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