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Porosity and pore size distribution in high-viscosity and conventional glass ionomer cements: a micro-computed tomography study
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Aline Borburema Neves, Laísa Inara Gracindo Lopes, Tamiris Gomes Bergstrom, Aline Saddock Sá da Silva, Ricardo Tadeu Lopes, Aline de Almeida Neves
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Restor Dent Endod 2021;46(4):e57. Published online October 29, 2021
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DOI: https://doi.org/10.5395/rde.2021.46.e57
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Abstract
PDFPubReaderePub
- Objectives
This study aimed to compare and evaluate the porosity and pore size distribution of high-viscosity glass ionomer cements (HVGICs) and conventional glass ionomer cements (GICs) using micro-computed tomography (micro-CT). Materials and MethodsForty cylindrical specimens (n = 10) were produced in standardized molds using HVGICs and conventional GICs (Ketac Molar Easymix, Vitro Molar, MaxxionR, and Riva Self-Cure). The specimens were prepared according to ISO 9917-1 standards, scanned in a high-energy micro-CT device, and reconstructed using specific parameters. After reconstruction, segmentation procedures, and image analysis, total porosity and pore size distribution were obtained for specimens in each group. After checking the normality of the data distribution, the Kruskal-Wallis test followed by the Student-Newman-Keuls test was used to detect differences in porosity among the experimental groups with a 5% significance level. ResultsKetac Molar Easymix showed statistically significantly lower total porosity (0.15%) than MaxxionR (0.62%), Riva (0.42%), and Vitro Molar (0.57%). The pore size in all experimental cements was within the small-size range (< 0.01 mm3), but Vitro Molar showed statistically significantly more pores/defects with a larger size (> 0.01 mm3). ConclusionsMajor differences in porosity and pore size were identified among the evaluated GICs. Among these, the Ketac Molar Easymix HVGIC showed the lowest porosity and void size.
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Web of Science
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Push-out bond strength of a self-adhesive resin cement used as endodontic sealer
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Eduardo Diogo Gurgel-Filho, Felipe Coelho Lima, Vicente de Paula Aragão Saboia, Tauby de Souza Coutinho-Filho, Aline de Almeida Neves, Emmanuel João Nogueira Leal da Silva
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Restor Dent Endod 2014;39(4):282-287. Published online August 20, 2014
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DOI: https://doi.org/10.5395/rde.2014.39.4.282
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Abstract
PDFPubReaderePub
- Objectives
The aim of the present study was to investigate the bond strength of RelyX Unicem (3M) to root canal dentin when used as an endodontic sealer. Materials and MethodsSamples of 24 single-rooted teeth were prepared with Gates Glidden drills and K3 files. After that, the roots were randomly assigned to three experimental groups (n = 8) according to the filling material, (1) AH Plus (Dentsply De Trey GmbH)/Gutta-Percha cone; (2) Epiphany SE (Pentron)/Resilon cone; (3) RelyX Unicem/Gutta-Percha cone. All roots were filled using a single cone technique associated to vertical condensation. After the filling procedures, each tooth was prepared for a push-out bond strenght test by cutting 1 mm-thick root slices. Loading was performed on a universal testing machine at a speed of 0.5 mm/min. One-way analysis of variance and Tukey test for multiple comparisons were used to compare the results among the experimental groups. ResultsEpiphany SE/Resilon showed significantly lower push-out bond strength than both AH Plus/Gutta-Percha and RelyX Unicem/Gutta-Percha (p < 0.05). There was no significant difference in bond strength between AH Plus/Gutta-Percha and RelyX Unicem/Gutta-Percha (p > 0.05). ConclusionsUnder the present in vitro conditions, bond strength to root dentin promoted by RelyX Unicem was similar to AH Plus. Epiphany SE/Resilon resulted in lower bond strength values when compared to both materials.
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