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EFFECT OF DENTIN SURFACE WETNESS ON TENSILE BOND STRENGTH OF SELF ADHESIVE RESIN CEMENTS

EFFECT OF DENTIN SURFACE WETNESS ON TENSILE BOND STRENGTH OF SELF ADHESIVE RESIN CEMENTS

Article information

Restor Dent Endod. 2009;34(2):113-119
Publication date (electronic) : 2009 January 14
doi : https://doi.org/10.5395/JKACD.2009.34.2.113
Department of Conservative Dentistry, College of Dentistry, Kangnung National University
*Corresponding Author: Kyung-Mo Cho, Department of Conservative Dentistry College of Dentistry, Kangnung National University, 123 Chibyon-dong Gangwon-do, Korea, Tel: 82-33-640-2470 Fax: 82-33-642-6410 E-mail: drbozon@kangnung.ac.kr
Received 2008 December 31; Revised 2009 February 09; Accepted 2009 February 17.

Abstract

Abstract

The purpose of this study was to compare the tensile bond strength of several self-adhesive resin cements bonded to dentin surfaces with different wet conditions.

Three self-adhesive resin cements; Rely-X Unicem (3M ESPE, St. Paul, MN, USA), Embrace Wetbond (Pulpdent, Oakland, MA, USA), Maxcem (Kerr, Orange, CA, USA) were used. Extracted sixty human molars were used. Each self-adhesive resin cement was adhered to the dentin specimens (two rectangular sticks from each molar) in different wet conditions.

Tensile bond strength were measured using universal testing machine (EZ Test, Shimadzu corporation, Kyoto, Japan) at a crosshead speed of 1.0mm/min. After the testing, bonding failures of specimens were observed by Operative microscope (OPMI pro, Carl Zeiss, Oberkochen, Germany). T-test was used to evaluate the effect of dentin surface wetness. One-way ANOVA test was used to evaluate the tensile bond strength of self-adhesive resin cements in the same condition. Scheffe's test was used for statistical analyzing at the 95% level of confidence.

The result showed that wetness of dentin surface didn't affect tensile bond strength of self-adhesive resin cements and Maxcem showed the lowest tensile bond strength.

Figure 1.

Specimen preparation for tensile bond strength.

Figure 2.

Schematic drawing of moulds.

Composition of materials used in this study

Handling methods of the resin cement

Means of self-adhesive resin cements according to dentin wetness

Comparison between self-adhesive resin cements on dry group

Comparison between self-adhesive resin cements on wet group

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Article information Continued

Figure 1.

Specimen preparation for tensile bond strength.

Figure 2.

Schematic drawing of moulds.

Table 1.

Composition of materials used in this study

Group Composition
Rely-X Unicem Powder: glass powder, silica, calcium hydroxide, pigment,
   substituted pyrimidine, peroxy compound, initiator.
Liquid: methacrylated phosphoric ester, dimethacrylate,
   acetate, stabilizer, initiator
Embrace Wetbond urethane methacrylate monomer, mono-2-methacryloyloxy ethyl, glass filler,
BA-30, sodium fluoride
Maxcem GPDM, co-monomers(mono-, di-, tri-functional methacrylate monomers),
proprietary self-curing redox activator, stabilizer, camphorquinone, barium glass fillers,
fluoroaluminosilicate glass fillers, fumed silica

GDPM; Glycerol dimethacrylate dihydrogen phosphate

Table 2.

Handling methods of the resin cement

Group Procedure
Rely-X Unicem Activate the capsule for 2s and mix it for 10s (Rotomix, 3M ESPE)
Embrace Wetbond Mix and the base and catalyst though the automix dual-barrel syringe
Maxcem Mix the base and catalyst through the automix dual-barrel syringe

Table 3.

Means of self-adhesive resin cements according to dentin wetness

Resin cements Dentin surface n Mean(MPa) ± SD
Unicem Dry 20 2.51 ± 0.01
Wet 20 2.51 ± 0.01
Embrace Dry 20 2.46 ± 0.24
Wet 20 2.51 ± 0.01
Maxcem Dry 20 2.05 ± 0.58
Wet 20 2.13 ± 0.48

Table 4.

Comparison between self-adhesive resin cements on dry group

Table 5.

Comparison between self-adhesive resin cements on wet group