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The etching effects and microtensile bond strength of total etching and self-etching adhesive system on unground enamel

The etching effects and microtensile bond strength of total etching and self-etching adhesive system on unground enamel

Article information

Restor Dent Endod. 2004;29(3):273-280
Publication date (electronic) : 2004 May 31
doi : https://doi.org/10.5395/JKACD.2004.29.3.273
Department of Conservative Dentistry, College of Dentistry, Pusan National University, Korea.
Corresponding author: Bock Hur. Department of Conservative Dentistry, College of Dentisty, Pusan National University, 1-10 Ami-dong, Seo-gu, Pusan, 602-739, Korea. Tel: 82-51-240-7454, bhur@pusan.ac.kr

Abstract

The purpose of this study was to evaluate the etching effects and bond strength of total etching and self-etching adhesive system on unground enamel using scanning electron microscopy and microtensile bond strength test.

The buccal coronal unground enamel from human extracted molars were prepared using low-speed diamond saw. Scotchbond Multi-Purpose (group SM), Clearfil SE Bond (group SE), or Adper Prompt L-Pop (group LP) were applied to the prepared teeth, and the blocks of resin composite (Filtek Z250) were built up incrementally. Resin tag formation was evaluated by scanning electron microscopy, after removal of enamel surface by acid dissolution and dehydration. For microtensile bond strength test, resin-bonded teeth were sectioned to give a bonded surface area of 1mm2. Microtensile bond strength test was perfomed.

The results of this study were as follows.

1. A definite etching pattern was observed in Scotchbond Multi-Purpose group.

2. Self-etching groups were characterized as shallow and irregular etching patterns.

3. The results (mean) of microtensile bond strength were SM; 26.55 MPa, SE; 18.15 MPa, LP; 15.57 MPa. SM had significantly higher microtensile bond strength than SE and PL (p < 0.05), but there was no significant differance between SE and PL.

References

1. Buonocore MG. A simple method of increasing the adhesion of acrylic filling materials to enamel surfaces. J Dent Res 1955. 34849–853.
2. Van Meerbeek B, Perdigao J, Lambrechts P, Vanherle G. The clinical performance of adhesives. Review. J Dent 1998. 26(1)1–20.
3. Bouillaguet S, Gysi P, Wataha JC, Ciucchi B, Cattani M, Godin Ch, Meyer JM. Bond strength of composite to dentin using conventional, one-step, and self-etching adhesive systems. J Dent 2001. 2955–61.
4. Perdigão J, Lopes M. Dentin Bonding-Questions for the new millennium. J Adhes Dent 1999. 1191–209.
5. Torii Y, Itou K, Hikasa R, Iwata S, Nishitani Y. Enamel tensile bond strength and morphology of resin-enamel interface created by acid etching system with or without moisture and self-etching priming system. J Oral Rehabil 2002. 29(6)528–533.
6. Hannig M, Bock H, Bott B, Hoth-Hannig W. Intercrystallite nanoretention of self-etching adhesives at enamel imaged by transmission electron microscopy. Eur J Oral Sci 2002. 110(6)464–470.
7. Hayakawa T, Kikutake K, Nemoto K. Influence of self-etching primer treatment on the adhesion of resin composite to polished dentin and enamel. Dent Mater 1998. 14(2)99–105.
8. Hannig M, Reinhardt KJ, Bott B. Self-etching primer vs phosphoric acid: an alternative concept for composite-to-enamel bonding. Oper Dent 1999. 24(3)172–180.
9. Perdigao J, Lopes L, Lambrechts P, Leitao J, Van Meerbeek B, Vanherle G. Effects of a self-etching primer on enamel shear bond strengths and SEM morphology. Am J Dent 1997. 10(3)141–146.
10. Perdigao J, Geraldeli S. Bonding characteristics of self-etching adhesives to intact versus prepared enamel. J Esthet Restor Dent 2003. 15(1)32–41.
11. Kanemura N, Sano H, Tagami J. Tensile bond strength to and SEM evaluation of ground and intact enamel surfaces. J Dent 1999. 27523–530.
12. Ibarra G, Vargas MA, Armstrong SR, Cobbb DS. Microtensile bond strength of self-etching adhesives to ground and unground enamel. J Adhes Dent 2002. 4(2)115–124.
13. Friedl KH, Hiller KA, Schmalz G. Placement and replacement of composite restorations in Germany. Oper Dent 1995. 20(1)34–38.
14. Mjor IA, Qvist V. Marginal failures of amalgam and composite restorations. J Dent 1997. 25(1)25–30.
15. Opdam NJ, Roeters FJ, Feilzer AJ, Smale I. A radiographic and scanning electron microscopic study of approximal margins of Class II resin composite restorations placed in vivo. J Dent 1998. 26(4)319–327.
16. Kugel G, Ferrari M. The science of bonding: from first to sixth generation. Review. J Am Dent Assoc 2000. 131Suppl. 20S–25S.
17. Hayakawa T, Kikutake K, Nemoto K. Related Articles, Influence of self-etching primer treatment on the adhesion of resin composite to polished dentin and enamel. Dent Mater 1998. 14(2)99–105.
18. Retief DH. Clinical applications of enamel adhesives. Review. Oper Dent 1992. Suppl 544–49.
19. Pashley DH, Tay FR. Aggressiveness of contemporary self-etching adhesives. Part II: etching effects on unground enamel. Dent Mater 2001. 17(5)430–444.
20. Ripa LW, Gwinnett AJ, Buonocore MG. The 'prismless' outer layer of deciduous and permanent enamel. Arch Oral Biol 1966. 1141–48.
21. Whittaker DK. Structural variations in the surface zone of human tooth enamel observed by scanning electron microscopy. Arch Oral Biol 1982. 27(5)383–392.
22. Nathanson D, Bodkin JL, Evans JR. SEM of etching patterns in surface and subsurface enamel. J Pedod 1982. 7(1)11–17.
23. Cehreli ZC, Altay N. Effects of a non-rinse conditioner and 17% ethylenediaminetetraacetic acid on the etch pattern of intact human permanent enamel. Angle Orthodont 2000. 7022–27.
24. Mcintyre J. In : Mount GJ, Hume WR, eds. The nature and progression of dental caries. Preservation and Restoration of Tooth Structure 1998. London: Mosby Inernational Ltd; 9.
25. Itou K, Torii Y, Suzuki K, Inoue K. Adhesion of restorative resin to tooth-adhesion promotes by Liner Bond III. Adhesive Dent 1994. 12174.
26. Pashley DH, Carvalho RM. Dentine permeability and dentine adhesion. J Dent 1997. 25(5)355–372.
27. Gwinnett AJ. The ultrastructure of the "prismless" enamel of permanent human teeth. Arch Oral Biol 1967. 12381–388.

Article information Continued

Figure 1

The SEM photographs of resin replica using Scotchbond Multi-Purpose

Figure 2

The SEM photographs of resin replica using Clearfil SE Bond

Figure 3

The SEM photographs of resin replica using Adper Prompt L-Pop

Table 1

Composition of three dentin bonding systems

Table 1

Table 2

Procedures of bonding agent application

Table 2

Table 3

Microtensile bond strengths(MPa, Mean ± SD)

Table 3